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Progress of Solid Electrolytes and the Electrochemical Sensors

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Journal of Materials Science & Technology 1997年第3期13卷 173-178页

作者： Yanruo HONG(National lab. on Solid Electrolytes and Metallurgical Testing Techniques, university of Science and Technology {2.,{2. 100083, china) National lab. on Solid Electrolytes and Metallurgical Testing Techniques University of Science and Technology Beijing Beijing 100083 China

Four types of solid state electrochemical sensors and their general principles are introduced in the paper. The novel type-IV sensors developed in the last few years are emphasized to study hereafter. The ways to design new electrochemical sensors and the directions to develop new solid electrolytes for new electrochemical sensors are also discussed.

关键词： Li Ba Progress of Solid Electrolytes and the Electrochemical Sensors Wang

Late Mesozoic metamorphic core complexes: new constraints on lithosphere thinning in North china

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Progress in Natural Science:Materials International 2006年第6期16卷 633-638页

作者： LIU Junlai, GUAN Huimei, JI Mo and HU Ling (State Key laboratory of geological Processes and Mineral Resources,{2. university of geosciences, and Key laboratory of Lithosphere Tectonics and Lithoprobing Technology of Ministry of Education,{2. university of geosciences, beijing 100083,{2.) [a] State Key laboratory of geological Processes and mineral Resources China University of Geosciences Key Laboratory of Lithosphere Tectonics Beijing China [b] Lithoprobing Technology of Ministry of Education China university of Geosciences Beijing China

Metamorphic core complexes (mcc’s) are among the most prominent structural styles of lithosphere extension and thinning during late Mesozoic in North china. In this paper, the geometrical, kinematic and age characteristics of some of the mcc’s, e.g. Liaonan, Waziyu (Yiwulushan), Yunmengshan, etc., are discussed. Some common characteristics, such as kinematic polarity, geometric asymmetry, occurrence over a time span, scattered and isolated distribution, and progressive development, can provide direct constraints on the regional lithosphere extension and thinning in North china, which does not favor the prevailing plume model, a general de-lamination model or extensional collapse of overthickened orogenic crust. We argue that several aspects, such as the kinematic polarity at depths during lithosphere extension, gradual break-up of lithosphere plate, relationship between magmatism and regional extension, and coeval activity of mcc’s and Tan Lu fault, should be taken into consideration when constructing a more reasonable model for lithosphere extension and thinning in North china.

关键词： North china late Mesozoic metamorphic core complex lithosphere extension and thinning.

SHRIMP U-Pb dating and Hf isotopic analyses of Middle Ordovician meta-cumulate gabbro in central Qiangtang, northern Tibetan Plateau

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Science china Earth Sciences 2010年第5期53卷 657-664页

作者： ZHAI QingGuo1 WANG Jun1, LI Cai2.& SU Li3 1 Institute of Geology, Chinese Academy of geological Sciences, beijing 100037,{2. 2.College of Earth Sciences, Jilin university, Changchun 130061,{2. 3 The geological laboratory center and State Key laboratory of geological Processes and Mineral Resources,{2. university of Geo- sciences,{12.,{2. 1. Institute of Geology Chinese Academy of Geological Sciences Beijing 100037 China2. College of Earth Sciences Jilin University Changchun 130061 China3. The Geological Laboratory Center and State Key Laboratory of Geological Processes and Mineral Resources China University of Geosciences Beijing 100083 China

Metabasites consisting of metamorphic ultra-mafic rocks, cumulate gabbro, gabbro (diabase), basalt, and plagiogranite are exposed at the Taoxinghu area in central Qiangtang, northern Tibetan Plateau. Zircon SHRIMP U-Pb dating for the cumulate gabbro yields a weighted mean age of 467±4 Ma, which is the oldest and most reliable magmatic age in this area. Zircon 176Hf/177Hf ratios range from 0.2.2.15 to 0.2.2.57, with εHf(t) values of 5.02.0.2., indicating that the cumulate gabbro was mainly derived from the depleted mantle. In addition, geochemical data of metabasites suggest that they have similar characteristics to those in the mid-ocean ridge basalts (MORB). The Taoxinghu metabasites may represent the fragment of Early Paleozoic ophiolite in the "Central Uplift" of the Qiangtang, northern Tibetan Plateau.

关键词： Qiangtang cumulate gabbro SHRIMP dating Hf isotope

The crystal structure of (Fe_(4)Cr_(4)Ni)_(9)C_(4)

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Science china Earth Sciences 2005年第3期48卷 338-345页

作者： SHI Nicheng1, MA Zhesheng1, XIONG Ming1, DAI Mingquan1, BAI Wenji2. FANG Qingsong2. YAN Binggang2.& YANG Jingsui2.1. X-ray Diffraction laboratory, china {2. of geosciences, beijing 100083, china 2. Institute of Geology, Chinese Academy of geological Sciences, beijing 100037, china 1. X-ray Diffraction laboratory China University of Geosciences 100083 Beijing China 2. Institute of Geology Chinese Academy of Geological Sciences 100037 Beijing China

(Fe4Cr4Ni)9C4 is a metal carbide mineral formed by combination of Fe, Cr and Ni with C. It occurs in a chromite deposit in the Luobusha ophiolite, Tibet. Based on the determina- tion of its crystal structure, the empirical formula is (Fe4.12.r3.84Ni0.96)8.92.3.70 and the simplified formula is (Fe4Cr4Ni)4C9. The mineral is hexagonal with a = 1.38392.2. nm, c = 0.44690(9) nm, space group P63 m c, Z=6 and the calculated specific gravity Dx = 7.089 g/cm3. Fe, Cr and Ni occupy different crystallographic sites and their coordination numbers are approximately 12. forming an alternate stacking sequence of flat and puckered layers along the c axis. Some me- tallic atoms have a defect structure. The interatomic distances of Fe, Cr and Ni are 0.2.2.— 0.2.66 nm, and the distances between Fe, Cr, Ni and C are 0.1893—0.2.69 nm. The coordina- tion number of carbon is 6. It occurs in interstices of the metallic atoms Fe, Cr and Ni to form trigonal-prismatically coordinated polyhedra. These coordination polyhedra are linked with each other via shared corners or shared edges into a new type of metal carbide structure.

关键词： Luobusha of Tibet, metal carbide, crystal structure.

Experimental remolding on the caprock's 3D strain field of the Indosinian-Yanshanian epoch in Tongling deposit concentrating area

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Science china Earth Sciences 2005年第7期48卷 863-874页

作者： DENG Jun1,HUANG Dinghua2.WANG Qingfei1,WAN Li1,SUN Zhongshi3,YANG Liqiang1 & GAO Bangfei1 1. State Key laboratory of geological Processes and Mineral Resources,{2. university of geosciences,beijing 100083,{2. 2. Faculty of Earth Sciences,{2. university of geosciences,Wuhan 430074,{2. 3. Department of Earth Sciences,Jilin university,Changchun 130061,{2. State Key laboratory of geological Processes and Mineral Resources China University of Geosciences Beijing 100083 China Faculty of Earth Sciences China University of Geosciences Wuhan 430074 China Department of Earth Sciences Jilin University Changchun 130061 China

Based on field observations and rheology analysis, we perform one analogue experiment and remold the 3D structural frame of Tongling deposit concentrating area firstly. Then we disassemble and dialyze the 3D structures of the model using the methods of "slicing" and "stripping". A series of sliced planes vertical to the fold hinges show similar landscapes of that in the drill hole profiles. Meanwhile, layer stripping analysis indicates that the deformation features of each layer in the model are qualitatively analogical to those obtained from field observations. Through contrasting the 3D structure between the experimental model and the field phenomena, we verify the following 3D deformation features of the caprock in this area: (1) the Tongling area mainly consists of three series of NE S-typed fold groups; (2. in the uniform stress field, the incoherent folds universally develop in different positions, along different axes as well as in different strata; (3) the faults propagate upward which are mostly inter-bedded detachment faults, while the fold amplitudes decrease while going deeper; and (4) the folds and cleavages are highly developed in the Silurian System indicating that the deformation effect of the Indosin-ian-Yanshanian structural layer terminates at this layer, which suggests that the Silurian System is the crucial layer for the inversion between brittle and plastic deformation domains and the underlying strata are subject to the control of another deformation system with distinct properties.

关键词： Tongling deposit concentrating area Indosinian-Yanshanian epoch 3D structural frame of the caprock analogue experiment slicing and stripping analysis structural model.

Effect and mechanism of stresses on rock permeability at different scales

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Science china Earth Sciences 2006年第7期49卷 714-723页

作者： YIN Shangxian1 & WANG Shangxu2.1. Safety Engineering College, North china Institute of Science and Technology, Yanjiao, beijing 101601, china 2. Key laboratory of Geophysics Exploration, china university of Petroleum, beijing 100083, china 1. Safety Engineering College North China Institute of Science and Technology Yanjiao Beijing 101601 China 2. Key laboratory of Geophysics Exploration China University of Petroleum Beijing 100083 China

The effect of geo-stress fields on macroscopic hydro-geological conditions or micro-cosmic permeability of water-bearing media should follow some laws or principles. Cases study and tests show that: (1) At macro-geologic large scale, deformed and crashed rocks which were induced by geo-stress fields changing provided space for groundwater storage and flow. Groundwater adjusts water-bearing space and dilatants fractures by flowing and press transferring. Coupling of liquid and solid can be implemented for rocks and groundwater. Although tectonic fields witness several times of change and build-up in geological time, stress fields forming regional tectonic framework are coherent with seepage fields, orientation of the maximum horizontal stress demonstrates main seepage direc-tions. (2. At macro-geologic middle scale, zones of stresses changing sharply, quite low stresses, stress or shear concentration can be used to show locations and types of main fractures, zones of geo-stresses changing equably can be acted as normal base media zones of tri-porosity media. (3) At micro-geologic small scale, tri-porosity media include fractured rocks, porous rocks and capillary rocks. Investigations indicate that porosity or permeability is functions of effective stresses, and po-rosity or permeability changing rules of porous rocks with variation of effective stresses can be de-scribed as the index model, the model of power exponent functions is suitable for those of fractured rocks, the model of the second power parabola for capillary rocks. The porosity and permeability loss in fractured rocks, which are greater than that in porous rocks, are shown by calculation of effective compressive coefficient and closing pressure in cracks. The calculations can also explain the mecha-nism why porosity changes are always larger than permeability changes. It is proved by the thick wall cylinder theory that the second power parabola relation between porosity or permeability loss and effective

关键词： geo-stress fields, seepage fields, tri-porosity media, effective stresses, permeability, porosity,scale.

Experimental study on interaction between simulated sandstone and acidic fluid

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Petroleum Science 2009年第1期6卷 8-16页

作者： Zhang Yongwang Zeng Jianhui Yu Bingsong State Key laboratory of Petroleum Resource and Prospecting China University of Petroleum Beijing 102249 China Basin and Reservoir Research center China University of Petroleum Beijing 102249 China State Key laboratory of geological Processes and Mineral Resources China University of Geosciences Beijing 100083 China

In order to investigate the controlling mechanism of temperature, fluid and other factors on water-rock interaction in the diagenetic process, we performed a series of simulated experiments on the interaction between two kinds of fluids with different salinity and a composite mineral system （simulated sandstone）, which contains albite, K-feldspar and other minerals. The experimental results showed that acidity was the most important factor that affected the dissolution of minerals in the composite mineral system. The lower the pH value, the more easily the minerals dissolved. At the same pH value, the dissolution abilities of different acids for various mineral components were also different. Compared to hydrochloric acid （inorganic acid）, oxalic acid （organic acid） was more able to dissolve aluminosilicate minerals. However, the dissolution ability of oxalic acid for carbonate minerals was lower than that of hydrochloric acid. In the process of fluid-rock interaction, dissolution of feldspar was relatively complicated. Increase of temperature would accelerate the dissolution of feldspar. Under acidic conditions, albite had a higher dissolution rate than K-feldspar. K-feldspar could dissolve and convert into montmorillonite and kaolinite, while albite could dissolve and convert into kaolinite both at 40℃ and 80℃. Presence of organic acid, and decrease of pH value and water salinity were all favorable for the dissolution of feldspar, but weakened the ability to form clay minerals.

关键词： Fluid simulated sandstone dissolution static experiment

Macro-and microscopic mechanical behaviour of flow of coal samples experimentally deformed at high temperatures and pressures

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Chinese Science Bulletin 2005年第S1期50卷 59-66页

作者： LIU Junlai , YANG Guang & MA Rui State Key laboratory of geological Processes and Mineral Resources,{2. university of geosciences, beijing 100083,{2. Key laboratory of Lithosphere Tectonics and Lithoprobing Technology of Ministry of Education,{2. university of geosciences, beijing 100083,{2. College of Earth Sciences, Jilin university, Changchun 130061,{2. china Univ Geosci State Key Lab Geol Proc & Mineral Resources Beijing 100083 Peoples R China china Univ Geosci Minist Educ Key Lab Lithosphere Tecton & Lithoprobing Technol Beijing 100083 Peoples R China Jilin Univ Coll Earth Sci Changchun 130061 Peoples R China

Coal samples from Qinshui Basin, Shanxi, china are experimentally deformed at temperatures and confining pressures of 2.0 - 500℃and 2.0 - 500 Mpa, strain rate of 0.5×10-5/s and total strain of 10%. The vitrinite reflectance of the coal samples varies from 3.04 to 1.79. It is shown that the strengths of the deformed samples change obviously with coeval increasing temperatures and pressures (T/P). At the experimental range of T/P, the effects of increasing temperature predominate over that of increasing pressure. Microstructural analysis indicates a brittle to ductile transition under experimental T/P conditions from 2.0 to 300℃, and 2.0 to 300Mpa. Brittle deformation microstruc-tures include macroscopic fracture zones and penetrative fracture associations. Elongation, undulose or irregular extinction, deformation lamellae and dynamic recrystallization of grains are the main ductile deformation microstructures. The variation of deformation mechanisms of the experimentally deformed coal samples is related to both the components of coals and T/P conditions. At low T/P, fractures occur in both inertinite and vitrinite of the samples. At higher T/P, crystalline plastic deformations are observed in the inertinite only.

关键词： coal experimental deformation brittle to ductile transition.

The Late Paleozoic Lithofacies Palaeogeography of the Benxi and Taiyuan Formation Controls Coal Accumulation in Yuzhou,Henan china

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地学前缘 2009年第S1期16卷 144-145页

作者： Yang Jiao,Xunlian Wang china university of {2.(beijing),beijing 100083,china.

The significance of this paper is to understand the characteristics of Late Paleozoic depositional environment, lithofacies palaeogeography and its distribu- tion pattern in Henan Province,to resolve the issue of basi... 详细信息

关键词： lithofacies palaeogeography sedimentary cycle coal measures Benxi-Taiyuan Formation