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^(13)C NMR spectra of tectonic coals and the effects of stress on structural components

Science china Earth sciences 2005年第9期48卷 1418-1437页

作者： JU Yiwen1,2. JIANG Bo1, HOU Quanlin2. WANG Guiliang1 & NI Shanqin2.1. College of Mineral Resource and Geosciences, china University of Mining and Technology, Xuzhou 2.1008, china 2. Laboratory of Computational Geodynamics, College of Geosciences, graduate school of Chinese academy of sciences, beijing 100049, china 1. College of Mineral Resource and Geosciences China University of Mining and Technology 221008 Xuzhou China 2. Laboratory of Computational Geodynamics College of Geosciences Graduate School of Chinese Academy of Sciences 100049 Beijing China

High-resolution 13C Nuclear Magnetic Resonance (NMR) spectra of different kinds of tectonic coals were obtained using the NMR (CP/MAS+TOSS) method. On the basis of this, after simulation synthesis and division of spectra, the relative contents of carbon functional groups were calculated. Combined with results of Ro, max, XRD testing and element analysis, stress effects on the composition of macromolecular structures in tectonic coals were studied further. The results showed that Ro, max was not only the important index for describing coal rank, but was also effective for estimating the stress effect of tectonic coals. Under tectonic stress ac- tion, Ro, max was the most direct indicator of the coal structure and chemical components. Changes in the stacking Lc of the coal basic structure unit (BSU) and La/Lc parameters could distinguish the temperature and stress effects on metamorphic-deformed environments, and re- flected the degree of structural deformation. Therefore, on the whole, Lc and La/Lc can be used to index of the degree of structural deformation of tectonic coals. In different metamorphic and de- formed environments, different kinds of tectonic coals are formed under structural stress. The changes in characteristics of the macromolecular structure and chemical composition are such that as the increase in structural deformation becomes stronger, from the brittle deformation coal to ductile deformation coal, the ratio of width at the half height of the aromatic carbon and ali- phatic carbon peaks (Hfa/Hfal ) was increased. As carbon aromaticity was raised further, carbon aliphaticity reduced obviously and different compositions of macromolecular structure appeared as a jump and wave pattern except for in wrinkle structure coal, which might result chiefly from stress effects on the macromolecular structure of different kinds of tectonic coals. The macro- moecular changes of wrinkle structure coal are reflected mainly on physical structure. In the metamorphi

关键词： tectonic coal, NMR, macromolecular structure, chemical component, stress effect.

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Effects of the grain size distribution on the temperature-dependent magnetic susceptibility of magnetite nanoparticles

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Science china Earth sciences 2010年第7期53卷 1071-1078页

作者： ZHAO XiangYu1,2.& LIU QingSong1 1 Paleomagnetism and Geochronology Laboratory (SKL-LE), Institute of Geology and Geophysics, Chinese academy of sciences, {2. 10002., china 2.graduate University of Chinese academy of sciences, beijing 100049, china 1. Paleomagnetism and Geochronology Laboratory (SKL-LE) Institute of Geology and Geophysics Chinese Academy of Sciences Beijing 100029 China2. Graduate University of Chinese Academy of Sciences Beijing 100049 China

Magnetite is an important magnetic remanence carrier in natural samples and therefore is of great interest in paleo-, rock-, and environmental magnetism. The magnetic properties of magnetite depend on many factors, e.g., concentration and grain size distribution (GSD). In this study, we theoretically investigated the temperature-dependent susceptibility (TDS) of magnetite nanoparticles with a lognormal GSD. Results show that the TDS is affected highly by the GSD mainly in three aspects. Firstly, the unblocking process becomes smoother with the increase of distribution width, characterizing as a wider Hopkinson peak on the TDS curve. Secondly, the blocking temperature increases with the increase of the median diameter or/and the distribution width. Thirdly, the maximum susceptibility decreases with the increase of distribution width, and has a logarithmic function relation with the standard deviation of the distribution. As a case study, this model was further applied to the thermal products of the Chinese loess/paleosol samples to determine the granulometry of newly-formed magnetite upon heating based on TDS curves. The results demonstrate the fidelity and feasibility of this method to determine the GSD of nano-sized magnetic particles.

关键词： Néel theory temperature dependence of susceptibility grain size distribution

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A 12.bit multichannel ADC for pixel detectors in particle physics and nuclear imaging

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Science china(Technological sciences) 2010年第5期53卷 1208-1214页

作者： WEI Wei1,2.3,WANG Zheng1,3 & ZHAO JingWei1,3 1 Institute of High Energy Physics,Chinese academy of sciences,{2. 100049,china 2.graduate University of Chinese academy of sciences,{2. 100049,china 3 Key Lab of Nuclear Detection Technology and Nuclear Electronics of Chinese academy of sciences,{2. 100049,china 1. Institute of High Energy Physics Chinese Academy of Sciences Beijing 100049 China2. Graduate University of Chinese Academy of Sciences Beijing 100049 China3. Key Lab of Nuclear Detection Technology and Nuclear Electronics of Chinese Academy of Sciences Beijing 100049 China

Modern pixel detectors in nuclear and particle physics experiments and also in nuclear imaging,starve for highly integrated application specified integrated circuit(ASIC),whereas in china the study of ASIC still stays far away from practical *** lack of ASIC strictly limits the research and development of domestic high energy physics field.A 12.bit multichannel ADC designed for high density readout is introduced as a major candidate for solution.A precise model is discussed and the simulation fully agrees with the model,which indicates a key principle of *** is performed according to the given rule,and novel layout techniques are carried *** results in all aspects are also obtained,showing an excellent real performance,which satisfies the practical requirement.

关键词： application specified integrated circuit high density readout Wilkinson ADC multi-channel ADC

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CH_4 uptake flux of Leymus chinensis steppe during rapid growth season in Inner Mongolia,china

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Science china Earth sciences 2010年第7期53卷 977-983页

作者： GENG YuanBo1, LUO GuangQiang1,2.& YUAN GuoFu1 1 Institute of Geographic sciences and Natural Resources Research, Chinese academy of sciences, beijing 100101, china 2.graduate University of Chinese academy of sciences, beijing 100049, china 1. Institute of Geographic sciences and Natural Resources Research Chinese Academy of Sciences Beijing 100101 China2. Graduate University of Chinese Academy of Sciences Beijing 100049 China

The influence of near ground atmosphere CH4 concentration, soil water content, soil Eh, plants, soil temperature, and pH on CH4 uptake flux of Leymus chinensis steppe during rapid growth season was studied using field in-situ measurement in Xilin River basin of Inner Mongolia, china. The results showed that CH4 uptake flux was positively correlated with near ground atmosphere CH4 concentration and soil Eh but negatively correlated with soil water content. Precipitation may decrease the CH4 flux by increasing the soil water content. The average fluxes of three treatments during the observation period were 1.52.(natural conditions, 1.51 (aboveground plants were excluded), and 2.00 mg m?2.d?1 (all plants were removed), respectively. The difference between the CH4 flux of natural condition treatment and that of removing aboveground plants treatment is small, whereas the flux of removing all plants treatment is larger than the other two treatments. This means that the contribution of aboveground plants to CH4 uptake flux is smaller than that of roots or roots-removing process. CH4 uptake flux is not sensitive to soil temperature and the narrow-ranged soil pH (6.36–7.86). The Leymus chinensis steppe acts as a sink for CH4, and thus more studies should be focused on its affecting factors and related mechanisms.

关键词： CH4 uptake flux Leymus chinensis steppe affecting factors static opaque chamber/gas chromatography method

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Modeling and verifying Web services driven by requirements:An ontology-based approach

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Science in china(Series F) 2006年第6期49卷 792-820页

作者： HOU Lishan1,3,JIN ZHi1,2.& WU Budan1,4 1. academy of Mathematics and Systems Science, Chinese academy of {2., beijing 100080, china 2. Institute of Computing Technology, Chinese academy of {2., beijing 100080, china 3. Institute of Software, Chinese academy of {2., beijing 100080, china 4. graduate University of Chinese academy of {2., beijing 100049, china 1. academy of Mathematics and Systems Science Chinese Academy of Sciences Beijing 100080 China 3. Institute of Software Chinese Academy of Sciences Beijing 100080 China 2. Institute of Computing Technology Chinese Academy of Sciences Bejing 100080 China 4. graduate University of Chinese academy of {2. Beijing 100049 China

Automatic discovery and composition of Web services is an important research area in Web service technology, in which the specification of Web services is a key issue. This paper presents a Web service capability description framework based on the environment ontology. This framework depicts Web services capability in two aspects： the operable environment and the environment changes resulting from behaviors of the Web service. On the basis of the framework, a requirement-driven Web service composition model has been constructed. This paper brings forward the formalization of Web service interactions with π calculus. And an automatic mechanism converting conceptual capability description to the formal process expression has been built. This kind of formal specification assists in verifying whether the composite Web service model matches the requirement.

关键词： Web service environment ontology automatic composition π calculus formal verification.

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A mixed method for measuring low-frequency acoustic properties of macromolecular materials

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Science china(Physics,Mechanics & Astronomy) 2006年第6期49卷 729-739页

作者： LIU Hongwei1,YAO Lei1,3,ZHAO Hong1,3,ZHANG Jichuan2.3 & XUE Zhaohong2.1. National Key Laboratory of Acoustics,Institute of Acoustics,Chinese academy of sciences,{2. 100080,china 2. Institute of Chemistry,Chinese academy of sciences,{2. 100080,china 3. graduate University of Chinese academy of sciences,{2. {12.,china National Key Laboratory of Acoustics Institute of Acoustics Chinese Academy of Sciences Beijing 100080 China Institute of Chemistry Chinese Academy of Sciences Beijing 100080 China graduate University of Chinese academy of {2. Beijing 100049 China

A mixed method for measuring low-frequency acoustic properties of macro-molecular materials is presented. The dynamic mechanical parameters of materials are first measured by using Dynamic Mechanical Thermal Apparatus(DMTA) at low frequen-cies,usually less than 100 Hz; then based on the Principles of Time-Temperature Super-position (TTS),these parameters are extended to the frequency range that acousticians are concerned about,usually from hundreds to thousands of hertz; finally the extended dynamic mechanical parameters are transformed into acoustic parameters with the help of acoustic measurement and inverse analysis. To test the feasibility and accuracy,we measure a kind of rubber sample in DMTA and acquire the basic acoustic parameters of the sample by using this method. While applying the basic parameters to calculating characteristics of the sample in acoustic pipe,a reasonable agreement of sound absorp-tion coefficients is obtained between the calculations and measurements in the acoustic pipe.

关键词： low-frequency acoustic properties,dynamic mechanical properties,Principles of Time-Temperature Superposition,acoustic pipe,sound absorption coefficient.

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Geographical Agglomeration of Chinese Manufacturing Industries

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中国人口·资源与环境：英文版 2007年第2期5卷 3-11页

作者： Zhang Hua 1, 2. Zheng Wei3 1. Institute of Geographical sciences and Natural Resources Research, Chinese academy of sciences, beijing 100101, china 2. graduate school of the Chinese academy of sciences, beijing 100039, china 3. school of Geography, beijing Normal University, beijing 100875, china Institute of Geographical sciences and Natural Resources Research Chinese Academy of Sciences Beijing 100101 China graduate school of the Chinese {2. of sciences Beijing 100039 China school of Geography Beijing Normal University Beijing 100875 China

Based on the plant level data from the First National Census of Basic Units, the Second National Census of Basic Units, and the First National Economic Census of china, this paper ex- amines the geographical agglomeration of Chinese manufacturing industries at a more disaggregated level both by industrial classi-fication and spatial unit analysis. Applying the agglomeration index proposed by Maurel and Sedillot, studies show that the most agglomerated industries are resource-intensive, and capital and technology intensive while industries demanding localized inputs or serving localized markets or favored by local governments are fairly dispersed. The more disaggregated industries are more spa- tially agglomerated. At the finer spatial scale, industries are more dispersed. Results indicate that within-county spillovers are stronger than nearby-county spillovers, and within-prefecture spillovers are stronger than nearby prefecture spillovers. Local- ized spillovers are still quite substantial at a range beyond that of counties. Comparing the agglomeration index of Chinese manu- facturing industries in 1996, 2.01 and 2.04, agglomeration seems to be a general tendency. Results also indicate that some industries have experienced remarkable changes in their levels of agglom- eration in the period 1996–2.04.

关键词： industrial agglomeration manufacturing industries the MS index

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Synthesis of well-defined functional PE graft copoly-mers via ATRP process

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Science Bulletin 2005年第10期50卷 1048-1051页

作者： CAO Chengang1, 2. DONG Jinyong1 & HU Youliang1 1. CAS Key Laboratory of Engineering Plastics, Joint Laboratory of Polymer Science and Materials, Institute of Chemistry, Chinese academy of sciences, {2. 100080, china 2. graduate school, Chinese academy of sciences, {2. 100039, china CAS Key Laboratory of Engineering Plastics Joint Laboratory of Polymer Science and Materials Institute of Chemistry Chinese Academy of Sciences Beijing 100080 China graduate school Chinese Academy of Sciences Beijing 100039 China

In summary, we have demonstrated a convenient yet highly efficient method forthe preparation of PE-based graft copolymers via ATRP.. By introducing a small amount of styrenegroups into PE chains via the selective copolymerization of ethylene with 1,4-divinylbenzenecatalyzed by Et(Ind)_2.rCl_2.MAO, the multifunctional ATRP initiator of1-chloroethylbenzene-containing PE was readily achieved by a quantitative hydrochlorination reactionand was shown to be very effective for the initiation of graft polymerization of MMA and styrene toprepare structurally well-defined PE-based graft copolymers.

关键词： ATRP Synthesis of well-defined functional PE graft copoly-mers via ATRP process PE well

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Artificial coordinating field and its application to motion planning of robots in uncertain dynamic environments

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Science china(Technological sciences) 2004年第5期47卷 577-594页

作者： JING Xingjian1, 2. WANG Yuechao1 & TAN Dalong1 1. Robotics Laboratory, Shenyang Institute of Automation, Chinese academy of sciences, Shenyang 110016,{2. 2. graduate school, Chinese academy of sciences, beijing 100039,{2. Correspondence should be addressed to Jing Xingjian 1. Robotics Laboratory Shenyang Institute of Automation Chinese Academy of Sciences 10016 Shenyang China 2. graduate school Chinese Academy of Sciences 10039 Beijing China

Artificial coordinating fields (ACF) are proposed to deal with the motion planning problems of mobile robots in uncertain dynamic environments. An ACF around an obstacle can generate two orthogonal force vectors to a robot: one is called the coordinating force vector which is purposively designed in this paper, and the other is the repulsive force vector which is the same as that in a conventional artificial potential field. The ACF is designed according to the updated motion purpose and the relative states of the robot with respect to its local environment, and it also satisfies the robot’s dynamic constraints. The direction of the coordinating force can be determiend on line according to an optimal evaluation function. The ACF can effectively remove the local minima, and reduce the oscillation of the planned trajectory between multiple obstacles. Only local knowledge of the environments is needed in the ACF-based motion planning. The properties of the ACF such as controllability, adaptability, safety and reachability are studied and discussed in detail in this paper. Theoretical analysis and simulations are given to illustrate our main results.

关键词： artificial coordinating fields, artificial potential fields, mobile robots, motion planning, uncertain dynamic environments.

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Applications of URANS on predicting unsteady turbulent separated flows

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Acta Mechanica Sinica 2009年第3期25卷 319-324页

作者： Jinglei Xu Huiyang Ma Department of Physics, graduate University of the Chinese academy of {2., 100049 beijing, china Department of Physics Graduate University of the Chinese Academy of Sciences 100049 Beijing China

Accurate prediction of unsteady separated turbulent flows remains one of the toughest tasks and a practi cal challenge for turbulence modeling. In this paper, a 2. flow past a circular cylinder at Reynolds number 3,900 is numerically investigated by using the technique of unsteady RANS （URANS）. Some typical linear and nonlinear eddy viscosity turbulence models （LEVM and NLEVM） and a quadratic explicit algebraic stress model （EASM） are evaluated. Numerical results have shown that a high-performance cubic NLEVM, such as CLS, are superior to the others in simulating turbulent separated flows with unsteady vortex shedding.

关键词： URANS Nonlinear eddy viscosity turbulencemodel ,Separated flows Circular cylinder

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