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Investigation of 'chazi'(damaged-enamels)on Chenghua doucai Porcelains

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science china(Technological sciences) 2009年第6期52卷 1722-1729页

作者： DU Feng1 & SU BaoRu2.1 Institute of Chemistry & Molecular engineering,Qingdao university of {2. & technology,Qingdao,china 2.college of Information {2. & technology,Qingdao university of {2. & technology,Qingdao,china Institute of Chemistry & Molecular engineering Qingdao University of Science & Technology Qingdao China college of Information science & {2. Qingdao University of Science & Technology Qingdao China

At the end of the 1950s,Sun Yingzhou considered that the 'chazi'(damaged colour)on Chenghua doucai imperial porcelain as a defect was originally produced in firing process during Chenghua period(1465―1487).Researchers in china have accepted his *** any fragment with the 'chazi' has never been found in several tons of Chenghua imperial sherds excavated from Ming imperial kiln site in *** china,few scholars have questioned the formation of 'chazi',and further investigated *** researchers at the Research Laboratory in the British Museum,employing unde-structive EDXRF,have analyzed the chemical composition of the 'chazi'(damaged colour)on a Chen-ghua doucai stem cup in the museum,and they have confirmed that the 'chazi'(damaged colour)was caused by the fire of the Jianfu palace in the Forbidden City in *** on their research,the authors studied the colour chemical principle of the 'chazi's' formation *** to the ceramic {2. principle,scientific reasoning for the 'chazi' was carried *** the help of the history of Qing court,the brainteaser of the 'chazi' was totally uncovered,the misunderstanding for the 'chazi' has also been *** research also suggests that employing modern science and {2. is a direction to study Chinese ancient ceramic further.

关键词： Chenghua doucai porcelains court eunuchs the set on fire at the Jianfu palace ’chazi’(damaged-enamels) the British Museum colour chemical principle archaeology using science and technology

Interactions of particles with solidifying front in Al_2._(3P) /Al Si composites

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中国有色金属学会会刊：英文版 1999年第3期9卷 524-529页

作者： Wu Shusen(吴树森), Huang Naiyu(黄乃瑜),An Ping(安萍) college of materials {2. and engineering, Huazhong university of {2. and technology, Wuhan 430074, P.R. china Huazhong Univ Sci & Technol Coll Mat Sci & Engn Wuhan 430074 Peoples R China

The behavior of ceramic particles at the solid/liquid interface and the distribution of particles in metallic matrix composites was studied with a zone unidirectional solidification method. Two kinds of partice dispersed composites, Al 2. 3P /Al 12.6%Si Sr and Al 2. 3P /Al 12.6%Si Sr Ca containing Al 2. 3 particles in volume fraction 2.～5% were used. In the Al 2. 3P /Al Si Sr composites, the particles were pushed by the solidifying front, and did not uniformly distribute in the solid. But in the Al 2. 3P /Al Si Sr Ca composites, the particles were engulfed by the solidifying front and uniformly distributed in the solid. The particles engulfing into the solid was realized only by Sr and Ca addition at the same time. As the interfacial energy between solid and particle was decreased in this case, the Al 2. 3 particles acted as the substrates of heterogeneous nucleation for the Si phases, which made the particles to be engulfed.

关键词： metallic matrix composites solidification particle size distributionDocument code: A

Comparison of the Molecular Interaction Volume Model with the Unified Interaction Parameter Formalism in the Fe-Cr-Ni Liquid Alloys at 1873 K

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Journal of materials science & {2. 2006年第4期22卷 559-564页

作者： Dongping TAO Faculty of materials and Metallurgical engineering, Kunming {2. of science and technology, Kunming 650093, china Faculty of materials and Metallurgical engineering Kunming University of Science and Technology Kunming 650093 China

The molecular interaction volume model (MIVM) for a general ternary system was deduced in detail for further clarifying and understanding its general multicomponent expression. Both MIVM and the unified interaction parameter formalism (UIPF) can be used to predict the activities of solutes and solvents in the Fe-Cr-Ni liquid alloys. But the former employs only the infinite dilute activity coefficients, and the later is not applicable without the dilute binary and ternary interaction parameters. MIVM has a certain physical meaning from the viewpoint of statistical thermodynamics, so it is an alternative for the estimation of activity coefficients of the solutes and solvents in a dilute or finite concentration metal solution where the interaction parameters are absent or their accuracies are questionable.

关键词： Activity Prediction Molecular interaction volume model Unified interaction parameter formalism

Sol-gel Preparation and Infrared Radiation Property of Boron-substituted Cordierite Glass-ceramics

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Journal of materials science & {2. 2010年第5期26卷 445-448页

作者： Shuming Wang and Fenghua Kuang School of materials science and {2.,university of science & technology Beijing,Beijing 100083,china [a] School of materials science and {2. university of science & {2. Beijing Beijing 100083 china

Boron for aluminum substitution in the cordierite structure has been examined by sol-gel preparation of different samples along the compositional junction Mg2.l4-xBxSi5O18 with x=0,0.5,1,*** increasing the x value from 0 to 1.5 the crystallization behavior changed *** amount B2.3 doping can promote the sintering of amorphous cordierite gel,effectively restrain the precipitation of μ-cordierite and enhance the crystallization of α-*** substitution of B3＋ for Al3＋ in cordierite crystal structure can effectively improve the near-infrared spectral emissivity of this cordierite based glass-ceramics.

关键词： Sol-gel Glass-ceramics Infrared radiation B3+ substitution Solid solution

Dry Friction Characteristics of Ti-6Al-4V Alloy under High Sliding Velocity

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Journal of Wuhan university of technology({2. science) 2007年第4期22卷 582-585页

作者：邱明 School of Mechatronic engineering Henan University of Science and Technology Theory of Lubrication and Bearing Institute Xi'an Jiaotong UniversityXi'an 710049China

Tribological behaviours of Ti-6Al-4V alloy pins sliding against GCr15 steel discs over a range of contact pressures （0.33-1.33 MPa） and sliding velocities （30-70 m/s） were investigated using a pin-on-disc tribometer under unlubricated conditions. The wear mechanisms and the wear transition were analyzed based on examinations of worn surfaces using SEM, EDS and XRD. When the velocity increases, the friction coefficient and the wear rate of the Ti-6Al-4V alloy show typical transition features, namely, the critical values of sliding velocities for 0.33 and 0.67 MPa are 60 and 40 m/s, respectively. The experimental results reveal that the tribological behaviours of Ti-6Al-4V alloys are controlled by the thermal-mechanical effects, which connects with the friction heat and hard particles of the pairs. A tribolayer containing mainly Ti oxides and V oxides is formed on the worn surface of Ti-6Al-4V alloy.

关键词： Ti alloy dry sliding friction behavior contact temperature wear mechanism

Dislocation Densites of Deformed Steel Sheets Based on Positron Annihilation

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International Journal of Minerals,Metallurgy and materials 1998年第1期12卷 47-50页

作者： Yonglin Kang Xianjin Wang (materials science and {2. School, university of science and technology Beijing, Beijing 100083, china) materials science and {2. School University of Science and Technology Beijing Beijing 100083 China

The variation regularity of dislocation densites of some deformed steel sheets under three kinds of strainpaths as uniaxial tension, plane strain and equal biaxial stretching was investigated by means of positron lifetimespectrum and Doppler-broadening techniques. The results show that the increasing rate of dislocation densites isrelated to the plastic strain path. A relationship between the increasing rate of micro-defects, macro-instability andforming limits during the process of steel sheet forming was got based on analyzing the mechanism of dislocationdensity increasing under different stress-strain condihons.

关键词： positron annihilation dislocation steel sheet strain path

Dynamic Mechanical Behaviour of Ultra-high Performance Fiber Reinforced Concretes

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Journal of Wuhan university of technology({2. science) 2008年第6期23卷 938-945页

作者：赖建中 Department of materials science & {2. Nanjing University of Science & Technology

Ultra-high performance fiber reinforced concretes （UHPFRC） were prepared by replacing 60% of cement with ultra-fine industrial waste powder. The dynamic mechanical behaviour of UHPFRC with different fiber volume fraction was researched on repeated compressive impact in four kinds of impact modes through split Hopkinson pressure bar （SHPB）. The experimental results show that the peak stress and elastic modulus decrease and the strain rate and peak strain increase gradually with the increasing of impact times. The initial material damage increases and the peak stress of the specimen decreases from the second impact with the increasing of the initial incident wave. Standard strength on repeated impact is defined to compare the ability of resistance against repeated impact among different materials. The rate of reduction of standard strength is decreased by fiber reinforcement under repeated impact. The material damage is reduced and the ability of repeated impact resistance of UHPFRC is improved with the increasing of fiber volume fraction.

关键词： ultra-high performance fiber reinforced concretes split Hopkinson pressurebar dynamic repeated impact

Three-Dimensional and Cross-sectional Characteristics of Normal Grain Growth Based on Monte Carlo Simulation

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International Journal of Minerals,Metallurgy and materials 1998年第3期12卷 129-133,139页

作者： Xiaoyan Song Guoquan Liu(Material science and engineering School, {2. of science and technology Beijing, Beijing 100083, china)(Department of materials science and engineering, Hebei {2. of technology, Tianjin 300130, china) Material science and engineering School University of Science and Technology Beijing Beijing 100083 China Departments of materials science and {2. Hebei University of Technology Tianjin 300130 China

An appropriate Monte Carlo method was developed to simulate the three-dimensional normal grain growth more completely. Comparative investigation on the three-dimensional and the cross-sectional characteristics of normal grain growth was done. It was found that the time exponent of grain growth determined from cross-section exhibits the same rule of increasing slowly with time and approaching the theoretical value n = 0.5 of steadygrain growth as the three-dimensional (3-D) system. From change of the number of grains per unit area with timemeasured in cross-section, the state of 3-D normal grain growth may be predicted. The gtain size distribution incross-section is different from that in 3-D system and can not express the evolution characteristic of the 3-D distribution. Furthermore, there exists statistical connection between the topological parameters in cross-section and thosein three-dimensions.

关键词： Monte Carlo simulation normal grain growth three-dimension cross-section characteristics

Magnetron sputtering synthesis of large area well-ordered boron nanowire arrays

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science china(Physics,Mechanics & Astronomy) 2004年第4期47卷 403-415页

作者： CAO Limin1,2. ZHANG Ze2.& WANG Wenkui1,2.1. Key Laboratory of Metastable materials science and {2. and college of materials science and engineering, Yanshan university, Qinhuangdao 066004, china 2. Institute of Physics, Chinese Academy of sciences, Beijing 100080, china 1. Key Laboratory of Metastable materials science and {2. and college of materials science and engineering Yanshan University 066004 Qinhuangdao China 2. Institute of Physics Chinese Academy of Sciences 100080 Beijing China

One-dimensionally nanostructured materials, such as nanowires and nanotubes, are the smallest dimensional structures for efficient transport of electrons and excitons, and are therefore critical building blocks for nanoscale electronic and mechanical devices. In this paper, boron nanowires with uniform diameters from 2. to 80 nm were synthesized by radio-frequency magnetron sputtering of pure boron powder and B2.3 powder mixtures in argon atmosphere. The boron nanowires produced stand vertically on the substrate surface to form well-ordered arrays over large areas with self- organized arrangements without involvement of any template and patterned catalyst. The high-density boron nanowires are parallel to each other and well distributed, forming highly ordered and uniform arrays. A more interesting and unique feature of the boron nanowires is that most of their tips are flat rather than hemispherical in morphologies. Detailed studies on its structure and composition indicate that boron nanowires are amorphous. Boron nanowire appears as a new member in the family of one-dimensional nanostructures. Considering the unique properties of boron-rich solids and other nanostructures, it is reasonable to expect that the boron nanowires will display some exceptional and interesting properties. A vapor-cluster-solid (VCS) mechanism was proposed to explain the growth of boron nanowires based on our experimental observations.

关键词： boron nanowires, magnetron sputtering, arrays, self-assembly.