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Synthesis and Structure of a 3-D organic-inorganic hybrid Copper(Ⅰ) iodide Complex:{[Cu2.2.Hgtsc)]·2.MF}n

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Synthesis and Structure of a 3-D organic-inorganic hybrid Co...

Research of Mechanism to System Flexibility Based on Embedded Real-time System

中国化学会第五届全国结构化学学术会议

作者： Wang Yun-Jie Li Hao-Hong Liu Ji-Bo Chen Zhi-Rong~* college of Chemistry and chemical {2.,Fuzhou university,Fuzhou,Fujian 350002.china.

A new copper(1)iodide coordination polymer[Cu)2.(Hgtsc)]·2.MF(1)(Hgtsc= glyoxal-thiosemicarbazone)has been synthesized via crystallization from DMF solution containing CuI,Nal·2.O and bidentate bridging ligand ***-crystal X-ray analysis reveals that 1 crystallizes in Monoclinic system,space group C2.c with cell parameters of α=

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Research of Mechanism to System Flexibility Based on Embedde...

PREPARATION OF NONIONIC WATER-SOLUBLE PHOSPHINES AND THEIR RHODIUM COMPLEXES FOR CATALYTC HYDROFORMYLATION OF OLEFIN

2.10 International Conference on Advanced Measurement and Test (AMT 2.10)

作者： Zhao guodong 1,a,Zhang guoyin 2.b,Yao aihong 3,c 1,2.3 college of Computer Science and Technology,Harbin engineering {2. Harbin,Heilongjiang,china,150001

This paper briefly describes the main ideas and coping strategies of mechanism to system flexibility based on embedded real-time system,designs the distributed system framework to system flexibility for the characteristics of embedded real-time *** building simulation testing environment based on RT-Linux real-time operating system,the impact of coping strategies of mechanism to system flexibility based on embedded real-time system and the distributed system framework to system flexibility on performance of RT-Linux was tested.

关键词： Flexible response,Embedded Operating System(EOS),Real-time System,RT-Linux

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Journal of Energy Chemistry 1994年第4期 436-441页

作者： YAN Yuan-Yong ZHUO Huan-Pei YANG Bo JIN Zi-Lincollege of chemical {2. Dalian university of Technology Dalian, Liaoning 116012

Two kinds of nonionic water-soluble phosphine complexes:tri（o-polyglycol ether phenyl） phosphine（Ⅰ） and tri（p-polyglycol ether phenyl）phosphine（Ⅱ）（n=3～12. were prepared. Their thodium complexes preparedin sitn were used in aqueous/organic solvent two-phase system for catalytichydroformylation of olefin. The results implied that the surfactant phosphineligands for the biphasic hydroformylation of olefin shows good catalytic activityand selectivity,At 100 C and 6.0 MPa total pressure （CO/H=1:1） theconversion of （?） dodecene and selectivity to aldehyde were higher than 85%.The effects of different conditions on the hydrofurmylation reaction wereexamined.

关键词： In PREPARATION OF NONIONIC WATER-SOLUBLE PHOSPHINES AND THEIR RHODIUM COMPLEXES FOR CATALYTC HYDROFORMYLATION OF OLEFIN IV than MPa

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溴化钠水溶液体系中煤的电化学脱硫

燃料化学学报 2003年第4期31卷 376-380页

作者：赵炜朱红朱英中国矿业大学化工学院江苏徐州221008 北方交通大学理学院北京100044

A suitable system and the best condition were determined for sulfur removal from coal by electrolysis through testing, and the effect of electrolytic conditions on desulfurization rate was studied At the same time, the influence of electrolysis desulfurization on the structure of coal was inquired into The results showed that the effect of desulfurization was the best in sodium bromide electrolytic system, the best desulfurization condition was =1 5?mol/L, I=0 7?A, T=343?K, t=4?h and the highest desulfurization rate reached 89% We found that with increasing electrolytic conditions, desulfurization rate increased at first, and then kept constant The analysis of IR spectrum showed that the structure of coal wasn’t

关键词：煤电化学脱硫脱硫率电解体系电解条件

CuO/γ-Al_2._3脱除烟气中SO_2.研究

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燃料化学学报 2003年第5期31卷 385-389页

作者：谢国勇刘振宇刘有智郭向云中国科学院山西煤炭化学研究所煤转化国家重点实验室山西太原030001 华北工学院化学工程系山西太原030051

将CuO γ Al2.3用于烟气脱硫研究。考查了脱硫剂制备参数及反应条件对CuO γ Al2.3脱硫活性的影响。并对不同载铜量的脱硫剂进行了XRD表征。结果表明,载铜量的质量分数为8%～10%时,脱硫剂具有较高的脱硫活性,高于10%的载铜量致使活性组... 详细信息

将CuO γ Al2.3用于烟气脱硫研究。考查了脱硫剂制备参数及反应条件对CuO γ Al2.3脱硫活性的影响。并对不同载铜量的脱硫剂进行了XRD表征。结果表明,载铜量的质量分数为8%～10%时,脱硫剂具有较高的脱硫活性,高于10%的载铜量致使活性组分CuO在Al2.3表面发生多层覆盖,活性位的利用率下降;在350℃～500℃的烟气温度及3000L kg·h～56000L kg·h的操作空速范围内,CuO γ Al2.3具有较高的脱硫活性,烟气中的O2.于CuO γ Al2.3的脱硫活性是必需的,水的影响不大。

关键词： CuO/γ—Al2.3 烟气脱硫

稀土在废水处理中的强化催化作用及其f轨道的贡献

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稀土 2010年第2期31卷 97-101页

作者：邝钜炽佛山科学技术学院化学与化工系广东佛山528000

论述了稀土在各种废水处理过程中发挥的强化催化作用。展望了掺杂稀土化合物能降低TiO2.带宽度,从而可使TiO2.解材料在太阳光下分解水中有机物成为可能,也有望提高TiO2.O3/UV的废水处理能力;最后指出稀土在废水处理中能够发挥超过一... 详细信息

论述了稀土在各种废水处理过程中发挥的强化催化作用。展望了掺杂稀土化合物能降低TiO2.带宽度,从而可使TiO2.解材料在太阳光下分解水中有机物成为可能,也有望提高TiO2.O3/UV的废水处理能力;最后指出稀土在废水处理中能够发挥超过一般过渡元素的催化作用,关键可能就在于其f轨道在成键过程中所作的贡献。

关键词：稀土废水处理光催化 f轨道

The New Calculation Method of Dynamic Feature of Gyro Motor Ball Bearing on Agricultural Machinery

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The New Calculation Method of Dynamic Feature of Gyro Motor ...

亚洲精细农业与计算机农业应用联合大会

作者： HUANG Qingxue 1 ZHAO Chunjiang 1 2.GE Shidong 3 1Department of material science and engineering Taiyuan university of Science and Tecchnology Taiyuan 03002. {2. 2.3} of Mechnaical Science and engineering Jilin university Changchun 13002. {2. 3Bearing research institute of Luoyang Luoyang 471039 {2.

The micromechanical gyroscope is the important seneor on agricultural machinery for course angle testing,and course angle is the key parameter for navigation positioning *** agricultural machinery on-stream is working under mal-cindition, so most of high degree accuracy fibre potic gyroscope not noly get bad Kalman filtering result under thrashing, vibration and temperature drift but also are expensive. The micromechanical gyroscope is extensively used in agricultural machinery navigation system because of its operating stationarity and bargain *** orientation performance of gyroscope is depend on the revolution stationarity and vibration of gyro motor,the anlysis and control of the revolution stationarity and vibration is based on the calculation of high-speed dynamic feature of gyro motor ball *** current calculation methods mostly use quasi statics method or quasi dynamics method .The quasi statics method based on the raceway control theory is not exact because of ingoring lubrication, so the error between inner and outer raceway control parameter is inevitable in the equilibriation equation of frictional force and gyro moment on rolling *** quasi dynamics method is not noly not fit for the feature of holder-oily lubrication but also complex. In this paper,based on the analysis of conventional calculation method about the dynamic character of high-speed rolling ball bearing , a new calculation method is put forward which simplifies the rolling ball under load at 3 direction into two hinge short bar according to the change features of the contact angle under high speed and the deformation of rolling ball and raceway. The specific form of stiffness matrix is given and the solving process by setting initial value of the load at three direction is discussesd. The complexity because of the variable coupling in the conventional Newton-Raphson method is avoid , and the congervence property is improved by this method, and the calculation forma

关键词： Agricultural machinery guidance gyroscope, Ball bearing dynamic feature, Calculation met hod

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离子液体复合溶剂法制备纤维素多孔微球

浙江大学学报（工学版） 2013年第12期47卷 2160-2164,2207页

作者：王鹏林东强姚善泾化学工程联合国家重点实验室浙江大学化学工程与生物工程学系浙江杭州310027

针对传统纤维素溶解方法的局限性,以离子液体1-丁基-3-甲基咪唑氯盐(BmimCl)和有机溶剂1,3-二甲基-2.咪唑啉酮(DMI)组成的复合溶剂溶解微晶纤维素,结合反相悬浮再生法,制备纤维素多孔微球.考察复合溶剂配比对纤维素溶解度和微球制备的影... 详细信息

针对传统纤维素溶解方法的局限性,以离子液体1-丁基-3-甲基咪唑氯盐(BmimCl)和有机溶剂1,3-二甲基-2.咪唑啉酮(DMI)组成的复合溶剂溶解微晶纤维素,结合反相悬浮再生法,制备纤维素多孔微球.考察复合溶剂配比对纤维素溶解度和微球制备的影响,比较分析了微球的理化性质,结果表明:所制微球体现出良好的球形度、孔度、孔径和比表面积;进一步选择合适微球,偶联离子交换配基,制备阴离子交换介质,体现出良好的蛋白吸附性能.采用复合溶剂法制备纤维素多孔微球,过程简便,性能优良,可以作为层析介质制备的新方法.

关键词：离子液体纤维素多孔微球 1-丁基-3-甲基咪唑氯盐 1,3-二甲基-2.咪唑啉酮

质子化程度对Anderson型抗肿瘤杂多酸[PtMo_6O_(2.)]^(8-)电子结构的影响

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四川大学学报（工程科学版） 2001年第6期33卷 50-54页

作者：向明礼袁支润肖慎修卢云四川大学化学工程学院四川成都610065 四川大学生物力学所四川成都610065 四川大学化学学院四川成都610064

运用密度泛涵理论中的离散变分方法 (DFT -DVM)对不同质子化程度的 [HxPtMo6O2.4]( 8-x) -(x =3.5、4 .5、6 )的电子结构进行了计算并对计算结果作了方差分析和F检验。结果表明 ,质子化程度的改变对原子静电荷 (除Mo原子电荷外 )、键级... 详细信息

运用密度泛涵理论中的离散变分方法 (DFT -DVM)对不同质子化程度的 [HxPtMo6O2.4]( 8-x) -(x =3.5、4 .5、6 )的电子结构进行了计算并对计算结果作了方差分析和F检验。结果表明 ,质子化程度的改变对原子静电荷 (除Mo原子电荷外 )、键级、HOMO、LUMO的组成、分子轨道能级以及态密度等 ,没有显著影响。根据计算和分析检验的结果推测 ,x =4 .5和x =6的Andeson平面型 [HxPtMo6O2.4]( 8-x) -也将具有抗肿瘤活性。

关键词：铂钼酸抗肿瘤活性电子结构密度泛函理论离散变分方法质子化程度 Andeson型抗肿瘤杂多酸