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Study on the coating of nano-scale SiO_2.film on the surface of nanocrystalline Mg-Al layered double hydroxides

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Science china Chemistry 2005年第2期48卷 107-114页

作者： ZHANG Zejiang1,2.3, MEI Xiujuan2. XU Chenghua1 & QIU Fali1 1. chengdu institute of Organic Chemistry, Chinese Academy of Sciences, chengdu 610041, china 2. Sichuan Fire Research institute of Public Security Ministry, chengdu 611830, china 3. Graduate School of the Chinese Academy of Sciences, Beijing 100039, china Correspondence should be addressed to Zhang Zejiang (email: zzjzzjzz@***) chengdu institute of Organic Chemistry Chinese Academy of Sciences Chengdu China Sichuan Fire Research institute of Public Security Ministry Chengdu China Graduate School of the Chinese Academy of Sciences Beijing China

The coating process of a nano-scale SiO2.film on the nanocrystalline Mg-Al layered double hydroxides via a sol-gel process was investigated. The uniform and dense SiO2.ilm with a thickness of about 5 nm on the nano-LDHs particles was characterized by the solubility test in the dilute HNO3 or HCl acid, TEM and FT-IR, XRD, TG and DSC. The chemical shifts of binding en- ergies of Al 2., Mg 2., Si 2. and O 1s on the coated particles indicate that the coating of the SiO2.nano-film on the surface of the nano-LDHs proceeds through the formation of Mg-O-Si and Al-O-Si bonds. The thermal analysis shows that both the SiO2.coated nano-LDHs and the nano-LDHs have a similar mass loss process, in which there are three obvious stages of mass loss in the temperature range of 40—700℃. Furthermore, the more the coatedamount of SiO2.n the surface of the nano-LDHs is, the less the mass loss of the samples is at 700℃.The nano- LDHs have two obvious endothermic peaks at 2.4.67℃ and 430.13℃, whose corresponding heat absorption capacities are 412.2. J/g and 336.30 J/g, respectively. In contrast, the coated nano-LDHs have only one endothermic peak at 2.3.60℃ with a heat absorption capacity of 2.1.2. J/g.

关键词： layered double hydroxides, nanocrystalline, silica, coating.

STRATIGRAPHIC AND DEPOSITIONAL FILLING MODEL OF NORTH TARIM FORELAND BASIN SYSTEM

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地学前缘 2000年第S1期7卷 340-341页

作者： Wang Longzhang[WT5,5”BX](chengdu institute of Geology and {2. resources, CGSA, chengdu 610082.china)

A stratigraphic and depositional filling modal of Triassic—Jurassic North Tarim foreland basin system is erected, through synthetic analysis of geological setting, depositional provenance, sequence stratigraphy, and quantitative tectonic stratigraphy. The result suggests that the major factors controlling formation and evolution of the system are oblique collision and convergence of different plates, and favorite hydrocarbon plays is *** geological setting analysis emphasizes the historical succession of the foreland basin system formation and evolution. The tectonic setting analysis sketchy outlines formation of the system and tectonic setting of its successive evolution. The sedimentary geology analysis reveals the uplift and subsidence of the basin basement a seesaw style movement.

关键词： foreland basin system filling model North Tarim Triassic and Jurassic

Identification of Hercynian shoshonitic intrusive rocks in central Hainan Island and its geotectonic implications

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Science Bulletin 2006年第20期51卷 2507-2519页

作者： XIE Caifu1, 2. ZHU Jinchu1, DING Shijiang3, ZHANG Yeming2. FU Tai’an2.& LI Zhihong2.1. State Key Laboratory for mineral Deposits Research and Department of Earth Sciences, Nanjing University, Nanjing 2.0093, china 2. Yichang {2. of Geology and mineral resources, Yichang 443003, china 3. Hainan Bureau of Geology and mineral resources, Haikou 5702.6, china State Key Laboratory for mineral Deposits Research and Department of Earth Sciences Nanjing University Nanjing China Yichang institute of Geology and mineral {2. Yichang China Hainan Bureau of Geology and mineral resources Haikou China

An identification has been made of some shoshonitic intrusive rocks in central Hainan Island recently. These rocks are K-rich (K2.=2.9%―5.1%, K2./Na2.=0.95―2.12., distinctly enriched in LILE and LREE, strongly depleted in Nb, Ta, and moder- ately depleted in Sr and Ti, with (87Sr/86Sr)i = 0.70859―0.7142. and ε Nd(t) = (?2.77―?7.49). They were derived from an EMⅡ-type mantle source. The enrichment process is related to metasomatism of depleted mantle caused by a great amount of fluid-melt released from oceanic crust and terri- genous sediments at great depth (eclogite facies) during the subduction of the South china plate under the Indochina-South china Sea plate in the Carbon- iferous–Early Permian. A SHRIMP U-Pb zircon dating yields a crystallization age of 2.2.7 Ma for the sho- shonitic intrusions, which is coeval with the strongly peraluminous granites found in central Hainan Island. These two kinds of rocks generally possess syn-intrusion ductile deformation structures. Thus they are considered to have been generated during the early stage (syn-thrust phase) of a post-collisional event. The primary magma of shoshonitic rocks was produced at a depth > 80 km by decompression- dehydration melting of previously enriched litho- spheric mantle wedge, phlogopite-bearing garnet peridotite, which was in turn caused by the break-off of a descendent slab and upwelling of a hot as- thenosphere. The rising of melts was accompaniedby crustal contamination and crystallization fractiona- tion (AFC). Combining with other related data, it is proposed that the southwards subduction and amal- gamation of the South china plate with the Indo- china-South china Sea plate took place at ca. 2.7- 2.8 Ma, which was a part of the convergence proc- ess of the Pangea supercontinent. The suture zone was probably located along the line of Song Ma-Beibu Gulf-north margin of the Yunkai Moun- tains-Wuyi Mountains.

关键词： SHRIMP U-Pb dating Hercynian shoshonitic intrusive rocks post-collisional event enriched mantle Hainan Island.

Trace element geochemistry of the Lower Cambrian black rock series from northwestern Hunan, South china

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Progress in Natural Science:Materials International 2004年第1期14卷 65-71页

作者： PAN Jiayong 1,2. *, MA Dongsheng 1 and CAO Shuanglin 1,2. (1.The State Key Laboratory for mineral Deposits Research, Nanjing University, Nanjing 2.0093, china 2. East china institute of Technology, Fuzhou 344000, china) Nanjing Univ State Key Lab Mineral Deposit Res Nanjing 210093 Peoples R China E china Inst Technol Fuzhou 344000 Peoples R China

Samples of black rock series collected from the Lower Cambrian Niutitang Formation, northwestern Hunan Province, china, were analyzed for trace elements. The trace element geochemical characteristics of the ore layer (high enrichments of Ni, Mo, V, U, Cu, Pb, Zn, Cd, Tl and Ba; high U/Th ratios and LREE enriched patterns with positive Eu and Y anomalies) support the assumption that the Ni Mo polymetallic layer is of submarine hydrothermal origin. High field strength elements (HFSE) and lithophile elements such as Nb, Ta, Zr, Hf, Li, Be, Rb, Cs, Th and Sc are remarkably higher in the upper unit than those in the lower unit of the Niutitang Formation. These features may reflect that hydrothermal contributions were diminished, and terrigenous constituents were increased in the sediments of the upper unit of the Niutitang Formation.

关键词： black rock series Early Cambrian trace elements northwestern Hunan china

The species diversity of fusulinaceans and high-frequency sea-level changes in the Carboniferous-Permian boundary section at Xikou, Zhen'an County,Shaanxi Province, china

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Science china Earth Sciences 2006年第7期49卷 673-683页

作者： ZHANG Haijun1, WANG Xunlian2. DING Lin1, XIA Guoying3 & WANG Lei2.1. institute of Tibetan Plateau Research, Chinese Academy of Sciences, Beijing 100085, china 2. Faculty of Earth Sciences and {2. resources, china University of Geosciences, Beijing 100083, china 3. Tianjin institute of Geology and {2. resources, Tianjin 300170, china institute of Tibetan Plateau Research Chinese Academy of Sciences Beijing China Faculty of Earth Sciences and mineral resources China University of Geosciences Beijing China Tianjin institute of Geology and mineral {2. Tianjin China

The study on the interrelation between sea-level changes and biodiversity with its evolu-tion has great significance for understanding the impact of global changes on organic evolution and exploring the inherent laws of life-environment coevolution in geological history. In this paper, the stratigraphic distribution of fusulinacean fauna in the Carboniferous-Permian boundary section at Xikou, Zhen’an County, Shaanxi Province, is analyzed quantitatively, and the relationship between the species diversity of fusulinaceans and relative sea-level changes is discussed. As a whole, the spe-cies numbers of fusulinacean fauna experience a rapid increase and an obvious decline in Xikou, Zhen’an County, from the Late Carboniferous to the Early Permian. There is a significant increase in species diversity around the Carboniferous-Permian boundary, which is one of the biggest bio-events of the fusulinacean fauna, and represents the radiation of Pseudoschwagerininae subfamily in the studied area. Integrated fusulinacean species diversity into sequence stratigraphic framework, de-tailed study suggests that the species diversity of the fusulinaceans is closely related to its relative stratigraphic location, and is essentially controlled by the sea-level changes, especially by the high-frequency sea-level changes. Generally, the species diversity of fusulinaceans is low, and the number of first and last appearance datum is small in the lower unit of high-frequency depositional cycle formed during the quick rise of the sea level; whereas the species diversity of fusulinaceans is high, and the number of first and last appearance datum is large in the upper unit of high-frequency cycle formed during the slow fall of the sea level. Within the third-order depositional sequence, the species diversity of the fusulinaceans at the first flooding surfaces and the maximum flooding surfaces is low, and it increases upward. The fusulinacean species diversity is low within the transgressive syst

关键词： fusulinaceans, species diversity, high-frequency cyclothem, sequence stratigraphy, sea-level changes, Carboniferous-Permian boundary, Zhen'an, Shaanxi.

Subsidence control and farmland conservation by solid backfilling mining technology

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中国有色金属学会会刊：英文版 2011年第S3期21卷 665-669页

作者： GUO Guang-li1, 2. FENG Wen-kai3, ZHA Jian-feng1, 2. 3, LIU Yuan-xu1, 2. WANG Qiang1, 2.1. Key Laboratory for Land Environment and Disaster Monitoring of the State Bureau of Surveying and Mapping, china University of Mining and Technology, Xuzhou 2.1116, china 2. Jiangsu Key Laboratory of {2. and Environmental Information Engineering, china University of Mining and Technology, Xuzhou 2.1116, china 3. State Key Laboratory of Geohazard Prevention and Geoenvironment Protection, chengdu University of Technology, chengdu 610059, china Key Laboratory for Land Environment and Disaster Monitoring of the State Bureau of Surveying and Mapping China University of Mining and Technology Xuzhou 221116 China Jiangsu Key Laboratory of resources and Environmental Information Engineering China University of Mining and Technology Xuzhou 221116 China State Key Laboratory of Geohazard Prevention and Geoenvironment Protection Chengdu University of Technology Chengdu 610059 China

Solid backfilling mining technology, which decreases the height of fissure zone and caving zone, and alleviates the subsidence, is a new technology for farmland conservation. Based on the situation analysis of farmland destruction in mining area, three ways for farmland protection were proposed. In order to improve the feasibility of this technology, the limited filling materials should be used to increase resources recovery ratio, and then the surplus materials could be backfilled into goaf. An index, namely farmland conservation ability, was put forward to optimize the ways for farmland conservation. At last, the Wanbei coal mine was taken as a case for farmland conservation. It was shown that 32.0 t dull coal was substituted and 52.hm2.farmland was conserved by solid backfilling mining in this coal mine.

关键词： solid backfilling farmland conservation mining subsidence equivalent mining height

SPACE-TIME TEXTURE AND TECTONIC EVOLUTION OF QAMDO BLOCK IN EAST TIBET

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地学前缘 2000年第S1期7卷 175-177页

作者： Wang Mingjie, Wang Gaoming[WT5,5”BX](chengdu institute of Geology and {2. resources,chengdu 610082.china)

Qamdo block in the east Tibet lay in front of southwestern margin of the Yangtze landmass and was one of many micro\|blocks between the Gondwana and the Eurasia continents .It played an important role in the development of the multi\|arc\|basin system of the north sector of the Jinsha\|lancang\|nujiang rivers . Space\|time texture of the block reflected the tectonic evolution of the east Tibet and neighbouring areas directly, providing important information for evolutionary history of the east Tethys.1\ Crustal structure of the Qamdo block\;Crustal structure of the Qamdo block is characterized by “double basement and double cover”.By double basement is meant the Middle—Upper Proterozoic crystalline basement and the Lower Paleozoic folded basement. The Middle—Upper Proterozoic crystalline basement is composed of medium\|high\|grade metamorphic biotite\|plagiogneiss, plagioclase\|amphibole schist, nacritid intercalated with (intermediate\|) basic metavolcanite. These rocks are characteristic of strong ductile deformed metamorphic core complex. The zircon of gneiss yields an U\|Pb age of 1680～2.00Ma while the basic metavolcanite give a Sm\|Nd age of *** Lower Paleozoic folded basement consists of the Lower Ordovician and Silurian. Basement of the Qamdo block is similar to that of the Yangtze landmass. By double cover we mean two covers consisting of the Upper Paleozoic and Mesozoic, respectively. The Upper Paleozoic is composed of carbonate and clastic rock which were formed from epicontinental to back\|arc basins. The Mesozoic consists of the Upper Triassic—Cretaceous concordant formations which were formed in a back\|arc foreland *** of the formations are molasse, neritic carbonate, paralic coal\|bearing rock and terrigenous red clastic rock from the bottom to the top.

关键词： East Tibet Qamdo block time\|space texture structural evol ution

Assessing the Carrying Capacity of Tourist Resorts: An Application of Tourists’ Spatial Behavior Simulator Based on GIS and Multi-Agent System

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Wuhan University Journal of Natural Sciences 2005年第4期10卷 779-784页

作者： ZHANG Ren-jun 1,2.1. institute of Mountain Hazards and Environment, Chinese Academy of Sciences, chengdu 610041, Sichuan, {2. 2. Graduated School of the Chinese Academy of Sciences, Beijing 100039, {2. institute of Mountain Hazards and Environment Chinese Academy of Sciences Chengdu Sichuan China Graduated School of the Chinese Academy of Sciences Beijing China

Based on the study of visitors' individual spatial behaviors, a tourists'spatial behavior simulator (TSBS) to assess the carrying capacity of tourist resorts was developed,TSBS employs GIS (Geographic Information System) to manage the spatial data,and Multi-Agent systemto simulate the actions of individual visitors. By utilizing TSBS, visitors' travel patterns such aslocation, cost, and state can be analyzed and predicted. Based on this analysis and prediction, themodel of assessing the carrying capacity of resorts is built. Our results show that TSBS will be aneffective tool to accurately assess the carrying capacity of tourist resorts.

关键词： tourist resort carrying capacity TSBS GIS Multi-Agent simulator

Encapsulation of inorganic particles by dispersion polymerization through ultrasonic irradiation

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Science china Chemistry 2005年第6期48卷 545-552页

作者： ZHANG Kai1,2. FU Qiang1, HUANG Yuhong2.& ZHOU Dehui2.1. College of Polymer Science and Engineering, Sichuan University, chengdu 610065, china 2. {2. of Structure Mechanics, china Academy of Engineering Physics, Mianyang 62.900, china College of Polymer Science and Engineering Sichuan University Chengdu China institute of Structure Mechanics China Academy of Engineering Physics Mianyang China

The nano-silica/polystyrene composite particles were prepared and characterized according to the following steps. First, the nano-silica particles were pretreated with surfactants under ultrasonic field. Second, the dispersion polymerization of styrene in a water/ethanol (1/6, weight ratio) medium, with poly(N-vinyl pyrrolidone) (PVP) as stabilizer and 2.2.-azobisizobu- tyronitrile (AIBN) as initiator in the presence of nano-silica particles was initiated with N2.purging through ultrasonic irradiation by taking its advantages of multieffect, i.e. dispersion, crushing, activation, and initiation. Finally, the polymerization kinetics characteristics were studied, and the encapsulation of composite particles was investigated with optical microscope, SEM, TEM, FTIR, X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC).

关键词： composite particle, dispersion polymerization, ultrasonic irradiation.