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Approaches to improving critical current density of YBCO superconducting thick films deposited by electrophoresis

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Science china(physics,Mechanics & Astronomy) 2004年第2期47卷 165-172页

作者： ZHU Yabin1,2. ZHOU Yueliang2. LIU Zhen2. WANG Shufang2. CHEN Zhenghao2. L?Huibin2. YANG Guozhen2. XIAO Ling3. REN Hongtao3. JIAO Yulei3.& ZHENG Minghui3.1. Department of physics, College of Science, Beijing Jiaotong University, Beijing 100044, china 2. Laboratory of Optical physics, institute of physics and center for {13. matter physics, chinese Academy of sciences, Beijing 100080, china 3. General Research {12. for Nonferrous Metals, Beijing 100088, china Correspondence should be addressed to Zhu Yabin (email: ybzhu@***) Department of physics College of Science Beijing Jiaotong University Beijing China Laboratory of Optical physics institute of physics and {2. for {3. matter physics Chinese Academy of Sciences Beijing China General Research institute for Nonferrous Metals Beijing China

Fabrication of YBCO superconducting thick films by electrophoresis has been widely reported. However, the value of critical current density (J c) is far from what the practical application requires. The superconducting thick films are obtained using top-seeded melt growth method with different proportional Y2.aCuO5 (Y2.1) addition. High-pressure oxygen has been used in the annealing process to improve the uniformity of the oxygen content in the superconducting thick films. When 40mol% Y2.1 powder is added to the YBa2.u3.7–5 (Y12.) powder,J c for the superconducting thick film by approaches described above reaches 7.008×103.A/cm2.(77 K, 0 T), which is greater than the value ever reported.

关键词： YBCO thick films, electrophoretic deposition, melt-textured.

The size effect on transport properties of colossal magnetoresistance materials La_(0.67)Ca_(0.3.)MnO_3

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Science china(physics,Mechanics & Astronomy) 2008年第3期51卷 251-257页

作者： LI PeiGang1,2.LEI Ming1,2.GUO YanFeng2.GUO Xi2.CHEN LeiMing2. TANG WeiHua1,2.SONG PengYun3.& CHEN JinPing3.1 Department of physics,center for Optoelectronics Materials and Devices,Zhejiang Sci-Tech University,Hangzhou 3.0018,{2. 2.National Laboratory for condensed matter physics,{13. of physics,chinese Academy of sciences,Beijing 100080,{2. 3.Department of physics,Peking University,Beijing 100875,{2. Department of physics Center for Optoelectronics Materials and Devices Zhejiang Sci-Tech University Hangzhou China National Laboratory for condensed matter {2. Institute of Physics Chinese Academy of Sciences Beijing China Department of physics Peking University Beijing China

High quality La0.67Ca0.3.MnO3.(LCMO) film was deposited via a novel pulsed electron deposition technique on SrTiO3.100) single crystal substrate. The micro-bridge with different widths was fabricated by using electron beam lithography (EBL) technique and their transport properties were studied. For the micro-bridges with width of 2.and 1.5 μm,the insulator-to-metal transition temperature (TP) keeps un-changed compared with the film. For the micro-bridges with width of 1 μm,the TP shifts towards the lower temperature by 50 K. When the width decreases down to 500 nm,the insulator-to-metal transition disappears. The magnetoresistance be-havior of these micro-bridges was studied,and the results show that the low field magnetoresistance (LFMR) decreases and the high field magnetoresistances (HFMR) keep almost unchanged as the width of micro-bridge is reduced.

关键词： colossal magnetoresistance pulsed electron deposition electron beam lithography electrical transport properties

An Explicit Function Expression for dc Bias and Temperature Dependence of Magnetoresistances in Magnetic Tunnel Junctions

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Journal of Materials Science & Technology 2002年第6期18卷 497-501页

作者： Xiufeng HANState Key Laboratory of Magnetism, institute of physics and center of {2. {3. physics, chinese Academy of sciences, Beijing 100080, china chinese Acad Sci Inst Phys State Key Lab Magnetism Beijing 100080 Peoples R China chinese Acad Sci Ctr Condensed Matter Phys Beijing 100080 Peoples R China

An explicit function expression for the bias voltage or/and temperature dependences of tunnel magnetoresistance ratio and resistances were obtained with a unique set of intrinsic parameters. Two of these intrinsic parameters are the Curie temperature TC and the density of state (DOS) for itinerant majority and minority electrons ξ(ρM/ρm), which are the eigen parameters of ferromagnetic electrodes. Others are the spin-dependent matrix-element ratio (i.e., |Td|2.|TJ|2.) and the anisotropic-wavelength-cutoff energy ECγ of spin-wave spectrum in magnetic tunnel junction (MTJ), which are the structure parameters of an MTJ. These intrinsic parameters can be predetermined using the experimental measurement or, in principle, using the first-principle calculation method for an MTJ with the three key layers of FM/I/FM. Furthermore, a series of experimental data for an MTJ, for example, a spin-valve-type MTJ of Ta (5 nm)/Ni79Fe2.(2. nm)/lr2.Mn78(12.nm)/Co75Fe2.(4 nm)/AI(0.8 nm)-oxide/Co75Fe2.(4 nm)/Ni79Fe2.(2. nm)/Ta (5 nm) in this work, can be self-consistently evaluated and explained using such concise explicit function formulations.

关键词： Magnetic tunnel junction TMR Spin-electron transport Magnon excitation Spin-polarization Magnetotransport

Fluorescence dynamics of interactions between polyamide PyPyPyβDp and DNA

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Science china Chemistry 2006年第1期49卷 75-80页

作者： ZHANG Huijuan1,2. WANG Jin3. WU Yishi1, YUAN Gu3. AI Xicheng1, WANG Li4 & ZHANG Jianping1 1. State Key Laboratory for Structural Chemistry of Unstable and Stable Species, institute of Chemistry, chinese Academy of {2., Beijing 100080, china 2. School of Life Science and Technology, Beijing institute of Technology, Beijing 100081, china 3. College of Chemistry and Molecular Engineering, Peking University, Beijing 100080, china 4. center for condensed {13. {12., institute of physics, chinese Academy of {2., Beijing 100080, china Correspondence should be addressed to Ai Xicheng and Zhang Jianping State Key Laboratory for Structural Chemistry of Unstable and Stable Species Institute of Chemistry Chinese Academy of Sciences Beijing China School of Life Science and Technology Beijing Institute of Technology Beijing China College of Chemistry and Molecular Engineering Peking University Beijing China center for condensed {2. {3. Institute of Physics Chinese Academy of Sciences Beijing China

The photophysical properties of the polyamide PyPyPyβDp (PPP) were investigated by means of steady-state absorption and fluorescence spectroscopies, as well as time-resolved fluo-rescence spectroscopy. It was found that the excited-state properties of PPP are very sensitive to solvents. In TKMC buffer PPP exhibited weak fluorescence with a decay time constant of 16 ps, while with the decrease of the solvent polarity PPP showed the blue-shifted peak position, increased inten-sity and lengthened life-time for its fluorescence behavior. In the presence of calf thymus DNA, it was observed that the fluorescence intensity was enhanced and the fluorescence lifetime increased from 16 to 3.0}ps for PPP, which verified that PPP bound into the minor groove of DNA duplex.

关键词： polyamide (PPP), calf thymus DNA (ctDNA), time-resolved fluorescence spectroscopy, recognition dynamics.

High-pressure synthesis and properties of CeO_2.ZrO_2.solid solution

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chinese Science Bulletin 2001年第10期46卷 801-806页

作者： XU Dapeng, WANG Quanyong, LU Zhe, LIU Zhiguo, ZHANG Gongmu & SU Wenhui1. Department of physics, Jilin University, Changchun 13.02. china 2. International {2. for Materials physics, chinese Academy of sciences, Shenyang 110015, china 3. {2. for condensed matter and Radiation physics, china {2. of Advanced Science and Technology (World Laboratory), Beijing 100080, china Department of physics Jilin University Changchun China International center for Materials physics Chinese Academy of Sciences Shenyang China center for condensed {2. and Radiation {3. China Center of Advanced Science and Technology (World Laboratory) Beijing China

Using nanoparticles of CeO2.and ZrO2.prepared by the chemical precipitation method as starting materials, the single-phase cubic Ce0.5Zr0.5O2.solid solution (c-Ce0.5Z0.5O2. has been synthesized under 3.1 GPa at 1073.K for the first time. The structure of the c-Ce0.5Zr0.5O2.has not been changed before and after annealing at 773.K for 1 h. Only an unknown EPR signal (g =1.990) has been observed in the c-Ce0.5Zr0.5O2.and not varied after annealing at 773.K for 1 h, which exhibited that there exists no Ce3. in the c-Ce0.5Zr0.5O2.and the Ce4+ has not been reduced into Ce3. after annealing. The transport mechanism is ionic for the c-Ce0.5Zr0.5O2. The bulk conductivity (a =1.2.10-5 S/cm at 82. K, σ=2.1 ×10-3.S/cm at 112. K) is the same as that of CeO2. but smaller than that of Y2.3.stabilized ZrO2. A marked curvature at T = 82. K has been observed in the Arrhenius plot of the bulk conductivity. The activation energy below 82. K is lower than that above 82. K, and the reason has been discussed.

关键词： CeO2.ZrO2 nanocrystalline high-pressure and -temperature solid-state reaction solid solution.

Containerless solidification of Zr_(41)Ti_(14)Cu_(12.5)Ni_(10)Be_(2..5) glass-forming alloy in drop tube

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chinese Science Bulletin 2002年第20期47卷 1700-1703页

作者： LI Gong, SUN Liling & WANG WenkuiCollege of Material sciences and Engineering, Yanshan University, Qinhuangdao 066004, china {2. for {3. matter physics, institute of physics, chinese Academy of sciences, Beijing 100080, china National Microgravit Coll. of Mat. Sci. and Engineering Yanshan University Qinhuangdao 066004 China center for condensed {2. {3. Institute of Physics Chinese Academy of Sciences Beijing 100080 China National Microgravity Laboratory Chinese Academy of Sciences Beijing 100080 China

Droplets of Zr41Ti14Cu12.5Ni10Be2..5 glass forming alloys with different sizes are solidified in a drop tube containerless processing. Glass transition behavior, crystallization kinetics, and the phase evolution during annealing of the Zr41Ti14Cu12.5Ni10Be2..5 glassy spheres are investigated. The experimental results indicate that the apparent activation energy of the glass transition (Eg=43..5 kJ/mol), and the activation energy of the main crystallization reaction (Ep1 = 2.9.6 kJ/mol) are obviously different from those of bulk glass samples prepared by water quenched (Eg=559.1 kJ/mol and Ep1=192.5 kJ/mol). The difference is discussed in the view point of the atomic configuration of the liquid state of the metallic glass and nucleation mechanism.

关键词： ZrTiCuNiBe alloy containerless processing activation energy drop tube.

Pressure-induced crystallite breaking in La_(0.7)Sr_(0.3.Mn_(0.9)Fe_(0.1)O_3.nanosolids

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chinese Science Bulletin 1998年第6期43卷 458-461页

作者： ZHENG Fanlei 1, 2. SUI Yu 1, 3. XU Dapeng 1 and SU Wenhui 1, 4 1. Department of physics, Jilin University, Changchun 13.02.,{3. 2. Changchun{2., chinese Academy of sciences, Changchun 13.02.,{3. 3. institute of Metal R Department of physics Jilin University Changchun Chinas Changchun institute of physics Chinese Academy of Sciences Changchun China institute of Metal Research Chinese Academy of Sciences Shenyang China International center for Materials physics Chinese Academy of Sceinces Shenyang China center for condensed {2. and Radiation {3. CCAST (World Lab.) Beijing China

In the compacting process of the La 0.7Sr 0.3.n 0.9Fe 0.1O 3.nanosolids under the pressure range of 0.0-4.5 GPa, the apparent pressure-induced crystallite breaking phenomenon in these nanosolids was observed. With increasing pressure up to 4.5 GPa, the average grain size decreases by 46% while the magnetization of nanosolids decrease by 40% and their coercive increases by 3.%. This kind of breaking has a close relation to the existence of oxygen deficiency in La 0.7Sr 0.3.n 0.9Fe 0.1O 3.nanoparticles. A simple and convenient method for preparing the bulk nanosolids with a large number of clean interfaces has been suggested.

关键词： nanosolid pressure-induced breaking high pressure.

Colossal magnetoresistive p-n junctions of perovskite oxide La_(0.9)Sr_(0.1)MnO_3.SrNb_(0.01)Ti_(0.99)O_3

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chinese Science Bulletin 2003年第13期48卷 1328-1330页

作者： L Huibin, DAI Souyu, CHEN Zhenghao, YAN Lei, ZHOU Yueliang & YANG Guozhen Laboratory of Optical physics, institute of physics & {2. for {3. matter physics, chinese Academy of sciences, 100080 Beijing, china Laboratory of Optical physics Center for Condensed Matter Physics Chinese Academy of Sciences 100080 Beijing China

We have successfully fabricated the colossal magnetoresistive (CMR) p-n junctions of perovskite oxide La0.9Sr0.1MnO3.SrNb0.01Ti0.99O3.(LSMO/SNTO) with laser molecular beam epitaxy. The I-V characteristics of the LSMO/SNTO p-n junctions as a function of applied magnetic field (05 T) were studied between 100 and 3.0 K. We found that the p-n junction exhibited the CMR behavior. The CMR ratio rR/R0 (rR = RH - R0) is positive in magnetic fields below 0.13.T and at high temperature, while it displays a negative CMR near 100 K and in magnetic fields over 0.13.T. The CMR ratio values are 8% at 0.1 T and 13. at 5 T and 3.0 K, 40% at 0.1 T and 150 K, 10% at 0.13.T and 60% at 5 T and 100 K. The CMR behavior of the p-n junction is different from those of the LaMnO3.compound family.

关键词：巨磁电阻钙钛矿氧化物 LSMO/SNTO CMR 激光分子束外延超导体

Studies of Structure Evolution of Nanostructured Hf_(11)Ni_(89) Alloy

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Journal of Materials Science & Technology 1998年第3期14卷 205-210页

作者： Zhenfu DONG and Lianmao PENG(Beijing Lab. of Electron Microscopy, institute of physics and center for {2. {3. physics,chinese Academy of sciences, P.O.Box 2.2., Beijing 100080, china)Ke LU and Zhuangqi HU(State Key Lab. for RSA, institute of Meta Beijing Lab. of Electron Microscopy Institute of Physics and Center for Condensed Matter Physics Chinese Academy of Sciences P.O.Box 2724 Beijing 100080 China State Key Lab. for RSA Institute of Metal Research Chinese Academy of Sciences Shenyang 110015 China

A nanostructured Hf11Ni89 ribbon sample was prepared by melt-spinning. It was found that the as-quenched sample is composed of a major HfNi5 compound nanophase and an interfacial magnetic Ni(Hf) solid solution phase. The structure evolution of the sample was studied by using X-ray difFraction (XRD), transmission electron microscopy (TEM), difFerential scanning calorimetry (DSC), resistivity and magnetothermal analysis. Upon heating, a second precipitation process of the Ni(Hf) phase prior to grain growth wa5 detected by means of both structural analysis and physical property measurements. The measurement results are discussed based on the relationship between microstructure and physical properties.

关键词： Studies of Structure Evolution of Nanostructured Hf Alloy Ni