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Identification of marine natural gases with different origin sources

Science china Earth Sciences 2008年第S1期51卷 148-164页

作者： WANG YunPeng 1 ,ZHAO ChangYi 2.,WANG ZhaoYun 2.,WANG HongJun 2.,TIAN Jin 1 ,ZOU YanRong 1 &LIU JinZhong1 1State Key Laboratory of Organic Geochemistry,Guangzhou {3. of Geochemistry,Chinese Academy of Sciences,Guangzhou 510640,china 2.0} of Geology,research {3. of Petroleum exploration and development,Petrochina,Beijing 100083.china State Key Laboratory of Organic Geochemistry Guangzhou Institute of Geochemistry Chinese Academy of Sciences Guangzhou 510640 China institute of Geology Research Institute of Petroleum Exploration and Development PetroChina Beijing 100083

Kinetic experiments of gas generation for typical samples of marine gas precursors including low-maturity kerogen,residual kerogen and oil as well as dispersed liquid hydrocarbon(DLH)in source rocks were performed by closed system,and the evolution trends of molecular and isotopic compositions of natural gases from different precursors against the maturity(R0%)at laboratory conditions were *** diagrams of gas origin were calibrated by using the experimental data.A diagram based on the ratio of normal and isomerous butane and pentane(i/nC4-i/nC5)was proposed and used to identify the origins of the typical marine natural gases in the Sichuan Basin and the Tarim Basin, *** the maturities of natural gases were estimated by using the statistical relationships between the gaseous molecular carbon isotopic data and maturities(δ13.-R 0 %)with different *** results indicate that the molecular and isotopic compositions of simulated gases from different precursors are different from each *** example,the dryness index of the oil-cracking gas is the lowest;the dryness indices of gases from DLH and kerogen in closed system are almost the same;and the dryness index of gases from residual kerogen is extremely high,indicating that the kerogen gases are very dry;the contents of non-hydrocarbon gases in kerogen-cracking gases are far higher than those in oil-cracking and DLH-cracking *** molecular carbon isotopes of oil-cracking gases are the lightest,those of kerogen in closed system and GLH-cracking gases are the second lightest,and those of cracking gases from residual kerogen are the *** calibration results indicate that the diagrams of ln(C1/C2.-ln(C2.C3.andδ13.2.δ13.3.ln(C2.C3.can discriminate primary and secondary cracking gases,but cannot be used to identify gas origin sources,while the diagram of i/nC4-i/nC5 can differentiate the gases from different *** application results of these diagrams show that gas mixtures ext

关键词： marine organic matter gas origin sources kerogen oil-cracking gas origin identification carbon isotope

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The crustal structure under Sanjiang and its dynamic implications:Revealed by seismic reflection/refraction profile between Zhefang and Binchuan,Yunnan

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Science china Earth Sciences 2005年第9期48卷 1329-1336页

作者： ZHANG Zhongjie1, BAI Zhiming1, WANG Chunyong2. TENG Jiwen1, Lü Qingtian3. LI Jiliang1, LIU Yifeng1 & LIU Zhenkuan4 1. institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing 10002.,{3. 2. institute of Geophysics,{3. Seismological Bureau, Beijing 100085,{3. 3. institute of Deposition Resource, Chinese Academy of Geosciences, Beijing 10003.,{3. 4. School of exploration and Information,{3. University of Geosciences, Beijing 100083.{3. 1. institute of Geology and Geophysics Chinese Academy of Sciences 100029 Beijing China 2. institute of Geophysics China Seismological Bureau 100085 Beijing China 3. institute of Deposition Resource Chinese Academy of Geosciences 100037 Beijing China 4. School of exploration and Information China University of Geosciences 100083 Beijing China

The fault belts in Sanjiang mainly include Jinshajiang-Honghe fault, Lancangjiang fault and Nujiang fault (called Sanjiang faults) in western Yunnan Province, china. By interpreting the wide-angle seismic reflection/refraction profile between Zhefang and Binchuan, which crosses Tengchong and Baoshan blocks in Dianxi (western Yunnan) tectonic zone, we recon- struct the crustal structure with seismic traveltime tomography for crustal P-wave velocity and the seismic scattering image for crustal seismic reflection structure. In this paper, we firstly present the crustal structure images of P-wave velocity and seismic reflection under the wide-angle seismic profile. These results demonstrate that, the crustal velocity structure and seismic reflec- tion structure along the profile can be divided into 3.segments, and there is an obvious difference of crustal structure among the eastern, the western and the middle segment. Generally, crustal P-wave velocities in the Baoshan segment are 0.1―0.2.km/s slower and seismic reflection am- plitudes from Moho discontinuity are stronger than the other 2.segments. In the studied area, crustal thickness is about 40 km, and shows the thickening tendency from west to east along the profile. Additionally, it can be seen that there is one strong-amplitude seismic reflection event as bright points at the depths of 8―10 km, along the segment of 80―115 km of the profile (south- ward of Tengchong); and seismic reflection wave-field from Moho discontinuity varies obviously along the lateral direction. Finally, we make some discussions on the crustal thickening pattern in the Sanjiang fault belt, structural environment of earthquake {3. and the contact rela- tionship between the Tengchong block, Banshan block and Luxi trough.

关键词： Sanjiang area wide-angle seismic profile crustal structure.

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Contributors and potential of hydrocarbon generation of source rocks by solid-state ^(13.C NMR spectroscopy

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Chinese Science Bulletin 1997年第6期42卷 478-481页

作者： WANGZhaoyun, ZHAO Changyi, CHENG Keming and LU Qinghua1. research institute of Petroleum {2. and {3., china National Petroleum Corporation, Beijing 100083. china:2. University of Petroleum, Beijing, 100083.4} research institute of Petroleum {2. and {3. China National Petroleum Corporation Beijing China University of Petroleum Beijing China

SOLID-STATE 13. nuclear magnetic resonance （NMR） technique is an effective method to study the texture of material. Under the condition of high magnetic field （400 MHz） and by the application of cross polarization... 详细信息

SOLID-STATE 13./sup>C nuclear magnetic resonance （NMR） technique is an effective method to study the texture of material. Under the condition of high magnetic field （400 MHz） and by the application of cross polarization, magic angle spinning （CP/MAS）, total sideband suppression （TOSS）, etc., the content of different textural carbons in kerogen has been quantitatively analyzed by the solid-state 13./sup>C NMR spectroscopy of a series of kerogen of thermal simulation samples with Ro value ranging from 0.64% to 1.76%. The results show that

关键词： solid 13. NMR analysis aliphatic carbon potential of hydrocarbon generation of source rocks.

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Biogas charging and dissipating process and its accumulation in the Sebei gasfield,Qaidam Basin,china

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Science china Earth Sciences 2008年第S1期51卷 36-44页

作者： JIN Qiang 1,CHENG FuQi 1,2.,SU AiGuo 3.,ZHU GuangYou 3.,WANG Li 1 &CAO Qian 1 1 china University of Petroleum,Dongying,Shandong 2.7061,{3. 2.Geological {2. of Shengli Oilfield,SINOPEC,Dongying,Shandong 2.7015,{3. 3.Petroleum exploration and development {2.,Petro{3.,Beijing 100083.{3. china Univ Petr Shandong 257061 Peoples R China SINOPEC Geol Inst Shengli Oilfield Shandong 257015 Peoples R China Petrochina Petr Explorat & Dev Inst Beijing 100083 Peoples R China

The Sebei gasfield is the largest biogas accumulation found in china and many reservoirs and seal rocks superposed on a syndepositional anticline in *** biogas charging and dissipating process and its distribution have been a research focus for many *** authors suggest a diffusing and accumulating model for the biogas,as they find that the shallower the gas producer,the more methane in the biogas,and the lighter stable carbon isotope composition of *** on the diffusing model,diffused biogas is quantitatively estimated for each potential sandy reservoir in the gasfield,and the gas charging quantity for the sandy reservoir is also calculated by the diffused gas quantity plus gas reserve in-place.A ratio of diffusing quantity to charging quantity is postulated to describe biogas accumulating state in a sandy reservoir,if the ratio is less than 0.6,the reservoir forms a good gas-pool and high-production layer in the gasfield,which often occurs in the reservoirs deeper than 900 m;if the ratio is greater than 0.6,a few gas accumulated in the reservoir,which frequently exists in the reservoirs shallower than 900 ***,a biogas accumulation model is built up as lateral direct charging from gas source for the sands deeper than 900 m and indirect charging from lower gas-bearing sands by diffusion at depth shallower than 900 *** this charging and diffusion quantitative model,the authors conducted re-evaluation on each wildcat in the central area of the Qaidam Basin,and found many commercial biogas layers.

关键词： biogas charging and diffusing model relative dissipated quantity Qaidam Basin

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The study on Sanmenxia annual flow forecasting in the Yellow River with mix regression model

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Science china(Technological Sciences) 2004年第z1期47卷 118-126页

作者： JIANG Xiaohui1, LIU Changming1,2. WANG Yu3.& WANG Hongrui1 1. Beijing Normal University, Beijing 100875, china 2. {3. of Geographic Science and Natural Resources, Chinese Academy of Sciences, Beijing 100101, china 3. Reconnaissance, Planning, Design and research {3., YRCC, Zhengzhou 450003. china Beijing Normal Univ Beijing 100875 Peoples R China Chinese Acad Sci Inst Geog Sci & Nat Resources Beijing 100101 Peoples R China YRCC Reconnaissance Planning Design & Res Inst Zhengzhou 450003 Peoples R China

This paper established mix regression model for simulating annual flow, in which annual runoff is auto-regression factor, precipitation, air temperature and water consumption are regression factors; we adopted 9 hypothesis climate change schemes to forecast the change of annual flow of Sanmenxia Station. The results show : (1) When temperature is steady, the average annual runoff will increase by 8.3. if precipitation increases by 10%; when precipitation decreases by 10%, the average annual runoff will decrease by 8.2.; when precipitation is steady, the average annual runoff will decrease by 2.4% if temperature increases 1℃; if temperature decreases 1℃, runoff will increase by 1.2.. The mix regression model can well simulate annual runoff. (2. As to 9 different temperature and precipitation scenarios, scenario 9 is the most adverse to the runoff of Sanmenxia Station of Yellow River; i.e. temperature increases 1℃ and precipitation decreases by 10%. Under this condition, the simulated average annual runoff decreases by 10.8%. On the contrary, scenario 1 is the best to the enhancement of runoff; i.e. when temperature decreases 1 ℃ precipitation will increase by 10%, which will make the annual runoff of Sanmenxia increase by 10.6%.

关键词： forecast annual flow, mix regression model, Sanmenxia Station

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Efficient computation of the compositional model for gas condensate reservoirs

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Communications in Nonlinear Science and Numerical Simulation 2000年第4期5卷 141-146页

作者： Jifu ZHOU, Jiachun LI and Jigen YE (institute of Mechanics, Chinese Academy of Sciences, Beijing 100080, china The {2. institute of Petroleum exploration and development, Beijing 100083. china) (Received December 2. 2.00) institute of Mechanics Chinese Academy of Sciences Beijing 100080 China Res. Inst. Petrol. Explor./Devmt. Beijing 100083 China

In this paper, a direct method, unsymmetric-pattern multifrontal factorization, for a large sparse system of linear equations is applied in the compositional reservoir model. The good performances of this approach are shown by solving the Poisson equation. And then the numerical module is embedded in the compositional model for simulating X15(3. gas condensate reservoir in KeKeYa gas field, Northwest china. The results of oil/gas reserves, variations of stratum pressure and oil/gas production, etc. are compared with the observation Good agreement comparable to COMP4 model is achieved, suggesting that the present model is both efficient and powerful in compositional reservoir simulations.

关键词： gas condensate reservoir compositional model sparse matrix

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Synthesis of GoldMag particles with assembled structure and their applications in immunoassay

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Science china Chemistry 2006年第6期49卷 534-540页

作者： CUI Yali1, ZHANG Lianying1, SU Jing1, ZHANG Caifeng3. LI Qi2. CUI Ting3. JIN Boquan2.& CHEN Chao1,3.1. Biochip research and {3. Center, Northwest University (National Engineering research Center for Miniaturized Detection System), Xi’an 710069, china 2. Department of Immunology, The Fourth Military Medical University, Xi’an 71003.0} china 3. Shaanxi Lifegen Co., Ltd., Xi’an 710069, china 1. Biochip research and development Center Northwest University (National Engineering Research Center for Miniaturized Detection System) Xi’an 710069 China 3. Shaanxi Lifegen Co. Ltd. Xi’an 710069 China 2. Department of Immunology The Fourth Military Medical University Xi’an 710032 China

Micrometer-sized Fe3.4 particles and nano-sized gold particles were first synthesized by methods of self-aggregation of surface-chemically modified Fe3.4 nanoparticles and citrate reduction of the Au3. to Au0, respectively. Interaction between these two types of particles resulted in the assembly of nano-sized gold particles on the surface of the micrometer-sized Fe3.4 particles, forming an assembled structure with the Fe3.4 core particles around which are attached nano-sized gold parti- cles. The Fe3.4/Au structure is named GoldMag particles with assembled structure. The synthetic process, structure, and magnetic property of the GoldMag particles were analyzed. GoldMag particles with assembled structure have an irregular shape, rough surface with a diameter of 2.3.μm. These particles exhibit the superparamagnetic property with saturated magnetization of 41 A·m2.kg. In a single step, antibodies could be readily immobilized onto the surface of the particles with a high binding capacity. The GoldMag particles can be used as a novel carrier in immunoassays. The maximum quantity of human IgG immobilized onto GoldMag particles was 3.0 μg/mg. In order to validate the quality of the GoldMag particles as immunoassay carriers, an immunoassay system was used. The relative amount of immobilized human IgG was measured by HRP-labeled anti human IgG. The coefficient of variation within parallel samples of each group was below 6% and the coefficient of variation of means between five groups carried out separately was below 7%. Based on the sandwich method, the Hepatitis B surface antigen (HBsAg) and interleukin-8 (IL-8) were also analyzed by qualitative and quantitative detection, respectively. The result indicated that the GoldMag particles with assembled structure were an ideal carrier in immunoassay.

关键词： GoldMag particles with assembled structure, synthesis, carrier, immunoassay.

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Natural gas origins of large and medium-scale gas fields in china sedimentary basins

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Science china Earth Sciences 2008年第S1期51卷 1-13页

作者： ZHANG ShuiChang &ZHU GuangYou research Center of research {2.s of Petro{3. exploration and development,Beijing 100083.{3. research Center of research {2.s of Petro{3. exploration and development Beijing 100083 China

china sedimentary basins present abundant natural gas resource thanks to its unique geological *** highly-matured hydrocarbon source rocks,widespread coal-measure strata and low temperature Quaternary saline strata,etc.,indicate the wide foreground of china natural gas resources. Up to now,most of the petroliferous basins have been discovered to have wholesale natural gas accumulation from Precambrian,Paleozoic,Mesozoic to Cenozoic in the east,the central,the west and the coast of *** large and medium-scale gas reservoirs are mainly composed of hydrocarbon gas with big dry coefficient,tiny non-hydrocarbon,wide carbon isotope distribution and varying origin types,the hydrocarbon gas includes coal-formed gas,oil-formed gas,biogenic gas and inorganic gas, ***-formed gas is the main type of china natural gas resources,in particular several explored large-scale gas fields(>100 billion cubic meter)of Kela {3.Sulige and Daniudi,etc.,they all belong to coal-formed gas fields or the gas fields consisting mostly of coal-formed ***-formed gas is also abundant in china marine basins,for example marine natural gas of Sichuan Basin generated from crude oil cracking *** and secondary biogenic gas fields were discovered respectively in the Qaidam Basin and Western Slope of Songliao *** addition,inorganic gases are mainly distributed in the eastern china,in particular the Songliao Basin with abundant carbon dioxide accumulation,indicating that the eastern china present large exploration potential of inorganic gas.

关键词： natural gas origin sedimentary basin large and medium-scale gas field

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Geological analysis and physical modeling of structural pumping in high effective formation of Kela 2.gas field

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Science china Earth Sciences 2006年第10期49卷 1070-1078页

作者： ZHAO Wenzhi1, WANG Hongjun1, SHAN Jiazeng2. WANG Zecheng1 & XU Dafeng1 1. research institute of Petroleum {2. and development, Petrochina, Beijing 100083. china 2. institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing 10002., china 1. research institute of Petroleum {2. and {3. Petrochina Beijing 100083 China 2. institute of Geology and Geophysics Chinese Academy of Sciences Beijing 100029 China

In a 3.D closed geological body, in case “structural expanding” inside is induced by stress, it can produce the pressure difference between the expanding cell and surrounding rock, then generate a pumping force directed toward the cell and accelerate the directional flow of fluid in the strata. The structural style and conditions of gas reservoir-formation in the kuqa depression are favorable to the structural pumping. According to similarity principle, a physical modeling of structure formation and gas filling process of the Kela 2.gas field has justified the occurrence of structural pumping and its important role in gas-reservoir formation with high efficiency under the compressive and well-sealed circumstance. Therefore, authors propose that structural pumping is an important mechanism of gas reservoir-formation with high efficiency in the kuqa depression.

关键词： Kela 2 gas field, structural pumping, gas-reservoir formation mechanism, high efficiency,physical modeling.

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Joint exploration of crustal structure in Fuzhou basin and its vicinities by deep seismic reflection and high-resolution refraction as well as wide-angle reflection/refraction

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Science china Earth Sciences 2005年第7期48卷 925-938页

作者： ZHU Jinfang1, XU Xiwei2. ZHANG Xiankang3. HUANG Zonglin1, CHEN Xiangxiong1, FANG Shengming3. LIU Baojin3. ZHENG Rongzhang2.4 1. Seismological Bureau of Fujian Province,Fuzhou 3.0003.china 2. institute of Geology,china Earthquake Administration,Beijing 10002.,china 3. research Center for exploration Geophysics,china Earthquake Administration,Zhengzhou 450002.china 4. State Key Laboratory of Earthquake Dynamics,institute of Geology,china Earthquake Administration,Beijing 10002.,china Seismological Bureau of Fujian Province Fuzhou 350003 China institute of Geology China Earthquake Administration Beijing 100029 China research Center for exploration Geophysics China Earthquake Administration Zhengzhou 450002 China State Key Laboratory of Earthquake Dynamics Institute of Geology China Earthquake Administration Beijing 100029 China

The Fuzhou basin and its vicinities are located at the northern end of the southeastern coastal seismic zone of the mainland of china. By the joint explorations of high-resolution seismic refraction and wide-angle reflection/refraction as well as deep seismic reflection in the region, which is the first synthetic profile in china, its fine velocity structure and geometric structure from the ground to Moho discontinuity is obtained. The result shows that the crust is obviously layered with a thickness of about 3.3.km. Basically, it consists of two parts: upper crust and lower crust. The velocity of the upper crust is 5.9-6.{3.km/s in which there is a 3.4-km-thick weak low-velocity layer between the depths of 10-15 km, while the velocity of the lower crust in the range of 6.3.7.{3.km/s. There exists a strong velocity gradient layer about 3.km thick above the Moho discontinuity whose velocity increases from 6.5 to 7.{3. km/s. There exist high-angle normal faults that are small in size and extend only in the shallow crust. These faults are the secondary developed on the hanging wall of westward dipping low-angle normal faults. Thus, their seismogenic ability is limited, however, there exists a high-angle deep fault in the crust from Changle-Zaoan fault zone to seashore fault zone. This deep fault has cut the interface between the upper and lower crusts and Moho discontinuity, and may be the deep structure to trigger destructive earthquake source in future to affect Fuzhou City. These results have advanced the detecting precision of the deep structure in the southeastern coastal seismic zone of the mainland of china. In the aspect of the combined feature of the deep and shallow extensional structures that consist of the westward dipping low-angle normal faults and secondary normal faults on their hanging walls in the upper crust, it is firstly obtained that a united structural interpretation has deepened the knowledge about the deep dynamic process in the southeastern coasta

关键词： deep seismic reflection high-resolution seismic refraction wide-angle.

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