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Electrical property of 8-mol% yttria-stabilized zirconia electrolyte by spark-plasma sintering

Science China(Technological Sciences) 2004年第5期47卷 569-576页

作者： JIAN Jiawen1,2. CHANG Aimin3, YANG Bangchao2.& ZHANG Yikang4.1. The School of Information Science Engineering, Ningbo university, Ningbo 3152.1, China 2. The School of Microelectronics and Solid-state Electronics, university of Electronic Science and Tech-nology of China, Chengdu 610054. China 3. The Xinjiang Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Urumqi 83002., China 4. Hongtak (Chengdu) Electronic Co., Ltd, Chengdu 61004., China Correspondence should be addressed to Jian Jiawen 1. The School of Information Science Engineering Ningbo University 315211 Ningbo China 2. The School of Microelectronics and Solid-state Electronics University of Electronic Science and Technology of China 610054 Chengdu China 3. The Xinjiang Technical Institute of Physics and Chemistry Chinese Academy of Sciences 830022 Urumqi China 4. Hongtak (Chengdu) Electronic Co. Ltd 610041 Chengdu China

Spark-plasma sintering (SPS) process was used to sinter ZrO2.(8Y) powders, and a relative density of 99% has been reached at a low temperature (1350°C) and short dwelling time (10 min) compared to the conventional sintered identical samples (14.0°C 4.h)(CS). By the X-ray diffraction (XRD) patterns, the microstructure of the SPS pellet and CS pellet are both indexed by the cubic unit cell (Fm3m). The finer crystallite size (D111) of the SPS pellet is 154.nm and D111 of the CS pellet is more than 1 μm. The AC impedance spectroscopy shows that the ionic conductivity of SPS pellet is different from that of CS pellet. The activation energy for the SPS ceramics, estimated from the slope in the range of 4.0–800°C, was 91 kJ mol?1, which is in good agreement with CS pellet (96 kJ mol?1), indicating that the conduction mechanism in SPS ceramics is similar to that in CS ceramics.

关键词： yttria-stabilized zirconia electrolyte, spark-plasma sintering, AC impedance.

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Biocompatibility evaluation in vitro. Part III: Cytotoxicity expression of human and animal osteoblasts on the biomaterials

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Journal of Central South university 2001年第3期13卷 147-155页

作者： RUAN Jian-ming 1,M.H. Grant 2.(1. State Key Laboratory for Powder Metallurgy, Central South university, Changs ha 4.0083, China 2. Bioengineering Unit, Strathclyde university, Glasgow, G4.0NW, UK) 1. State Key Laboratory for Powder Metallurgy Central South University 410083 Changsha China 2. Bioengineering Unit Strathclyde University G4 0NW Glasgow UK

Exclusion and inflammation in the clinic are observe d for various reas ons including material che- mical composition, physical properties as well a s macr o- and micro-structure of the implants, surface condition of the implants, and also patient dependent factors. Cytotoxicity expression of cells is a central issue i n current biocompatibility to screen the potential implant materials and drugs. This study was aimed at investigation reaction between the potential implant mat erials and surround tissue. Cytotoxicity of human and rat osteoblast in the mate rial extracts was determinated by testing standards such as GHS assay, MTT assay , alkaline phosphatase activity assay, LDH assay, and Lowry assay. Research resu lts demonstrated that compared with the control condition polystyrene culture pl a te both human and rat osteoblast cells have normal phenotypic expression in hydr oxyapatite extract, and this expression was statistically restricted in hydroxya patite-spinel extract. How- ever, this restrict, e.g. cytotoxicity could be partially eliminated by immersion treatment of the materials in culture medium.

关键词： biomaterial cytotoxicity biological molecular technique

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The steady-state solution of dendritic growth from the undercooled binary alloy melt with the far field flow

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Science China(Technological Sciences) 2009年第8期52卷 2280-2287页

作者： CHEN MingWen1,2. WANG ZiDong2.& XU JianJun2.3,4.1 School of Applied Sciences, university of Science and Technology Beijing, Beijing {4. China 2.School of Materials Science and Engineering, university of Science and Technology Beijing, Beijing {4. China 3 School of Mathematical Sciences, Nankai university, Tianjin 300071, China 4.Department of Mathematics and Statistics, McGill university, Montreal H3A 2.6, Canada School of Applied Sciences University of Science and Technology Beijing Beijing 100083 China School of Materials Science and Engineering University of Science and Technology Beijing Beijing 100083 China School of Mathematical Sciences Nankai University Tianjin 300071 China Department of Mathematics and Statistics McGill University Montreal H3A 2K6 Canada

The steady-state dendritic growth from the undercooled binary alloy melt with the far field flow is considered. By neglecting the interface energy, interface kinetics and buoyancy effects in the system, we obtaine the steady-state solution for the case of the large Schmidt number, in terms of the multiple variable expansion method. The changes of the temperature and concentration fields, the morphology of the interface, the normalization parameter and the Peclet number of the system induced by uniform external flow are derived. The results show that, compared with the system of dendritic growth from undercooled pure melt, the convective flow in the system of growth from undercooled binary alloy has stronger effects on the morphology of the interface. Nevertheless, the shape of the interface still remains nearly a paraboloid.

关键词： binary alloy melt convection dendritic growth interfaces steady-state solution multiple variable expansion method

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Test of magnetic susceptibility and grain-size age models of loess

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Progress in Natural Science:Materials International 2007年第11期17卷 1312-1317页

作者： Chen Yimeng1,2.3, Feng Zhaodong4.and Gong Huili1,2.1. MOE and Key Laboratory of Resources Environment and GIS of Beijing, Beijing 100037, China 2. Key Laboratory of 3D information Acquisition and Application, The Capital Normal university, Beijing 100037, China 3. Department of Economics & Management of Huizhou university, Huizhou 516007, China 4. Key Laboratory of Western China’s Environmental Systems, Ministry of Education, Lanzhou university, Lanzhou 730000, China) MOE and Key Laboratory of Resources Environment and GIS of Beijing Beijing 100037 China Key Laboratory of 3D information Acquisition and Application The Capital Normal University Beijing 100037 China Department of Economics & Management of Huizhou university Huizhou 516007 China Key Laboratory of Western China’s Environmental Systems Ministry of Education Lanzhou University Lanzhou 730000 China

Ages of the stratigraphic boundary MIS1/2.and MIS3/4.of the Yuanbu loess section in Linxia are used as the basis of the nodal control age. The age of MIS1/2.and MIS3/4.are obtained from the latest international research result—the climatic events recorded in the stalagmite in the Hulu Cave in Nanjing, that MIS1/2.is 11.5 kaB.P. and MIS3/4.is 59.8 kaB.P.. The ages of the two climatic events contain three nodal age control models (Model 1: 0 kaB.P.—59.8 kaB.P.; Model 2. 0 kaB.P.—11.5 kaB.P. and 11.5 kaB.P.—59.8 kaB.P.; Model 3: 11.5 kaB.P.—59.8 kaB.P.), which are used as the nodal control age separately. The deposition times of various stratigraphic horizons are calculated by using the magnetic susceptibility age model and grain-size age model, and then compared with each other. In addition, the AMS14. age, OSL age and the ages of YD and H events are compared with the ages of the corresponding horizons calculated by the three models of nodal control ages. From the analyses of lithologic characters and climatic stages it has been found that both the magnetic susceptibility age model and the grain-size age model have some defects. Because the accurate control ages are selected as the nodal points of the glacial period or interglacial period, the stratigraphic deposition times determined by the high resolution of magnetic susceptibility age model and grain-size age model approximate to the actual ages. As for the relative accuracy of the two age models, the magnetic susceptibility age model is more accurate than the grain-size age model.

关键词： loess nodal control age magnetic susceptibility age model grain-size age model test

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X-ray spectra induced in highly charged 4.Ar^q+ interacting with Au surface

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Science China(Physics,Mechanics & Astronomy) 2006年第2期49卷 203-212页

作者： ZHANG Xiao’an1,2. XIAO Guoqing1, YANG Zhihu1, CHEN Ximeng3, ZHAO Yongtao1, LI Fuli4. ZHANG Yinping1, CUI Ying3, ZHANG Hongqiang3, XU Xu3, SHAO Jianxiong3 & ZHAN Wenlong11. Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000, China 2. Department of Physics, Xianyang Normal university, Xianyang 712.00, China 3. Department of Modern Physics, Lanzhou university, Lanzhou 730000, China 4. Department of Applied Physics, Xi’an Jiaotong university, Xi’an 71004., China 1. Institute of Modern Physics Chinese Academy of Sciences Lanzhou 730000 China 2. Department of Physics Xianyang Normal University Xianyang 712000 China 3. Department of Modern Physics Lanzhou University Lanzhou 730000 China 4. Department of Applied Physics Xi’an Jiaotong University Xi’an 710049 China

By use of optical spectrum technology, the spectra of X-ray induced by highly charged 4.Arq+ ions interacting with Au surface have been studied. The results show that the argon Kα X-ray were emitted from the hollow atoms formed below the surface. There is a process of multi-electron exciting in neutralization of the Ar16+ion, with electronic con-figuration 1s2.in its ground state below the solid surface. The yield of the projectile Kα X-ray is related to its initial electronic configuration, and the yield of the target X-ray is related to the projectile kinetic energy.

关键词： highly charged ion hollow multi-electron excitation X- ray.

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Exotic structure of the third excited state in^(2.)Na

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Chinese Science Bulletin 2005年第23期50卷 2677-2680页

作者： LI Xihan1,2.3, LIANG Yujie1,2.3, DENG Fuguo1,2.3, LIU Zuhua1,4.& ZHOU Hongyu1,2.3 1. Key Laboratory of Beam Technology and Material Modification of Minister of Education, Beijing Normal {4., Beijing 100875, China 2. Institute of Low Energy Nuclear Physics, and Department of Material Science and Engineering, Beijing Normal {4., Beijing 100875, China 3. Beijing Radiation Center, Beijing 100875, China 4. China Institute of Atomic Energy, Beijing 102.13, China Key Laboratory of Beam Technology and Material Modification of Minister of Education Beijing Normal University Beijing 100875 China Institute of Low Energy Nuclear Physics and Department of Material Science and Engineering Beijing Normal University Beijing 100875 China Beijing Radiation Center Beijing 100875 China China Institute of Atomic Energy Beijing 102413 China

The probability of the last proton being out of the binding potential, P and the root-mean-square (rms) ra- dius (1/2. of the third excited state in 2.Na are calcu- lated by means of asymptotic normalization coefficie... 详细信息

The probability of the last proton being out of the binding potential, P and the root-mean-square (rms) ra- dius (2.1/2. of the third excited state in 2.Na are calcu- lated by means of asymptotic normalization coefficient (ANC) method with the experimental date existing. The results are P=54.73% and 2.1/2.5.2. fm respectively. The P value and the contribution of the asymptotic part to the 2.1/2.are compared with those of several other low energy states in 2.Na. It is found that the valence particle in the third excited state has an obvious larger P than those of other states. The density distribution of the valence proton in this state is also compared with the nucleons in the nuclear core 2.Ne, and a far extended tail can be seen clearly. These results show that the third ex- cited state in 2.Na is a proton halo state.

关键词：钠第三激发态外部结构有效半径密度分布渐近标准化系数

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HCWCI/Carbon Steel Bimetal Liner by Liquid-Liquid Compound Lost Foam Casting

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Journal of Iron and Steel Research International 2012年第10期19卷 13-19页

作者： XIAO Xiao-feng1,2. YE Sheng-ping2. YIN Wei-xin3, XUE Qiong4.(1. School of Mechanical Engineering and Automation, Wuhan Textile university, Wuhan 4.0073, Hubei, China 2. State Key Laboratory of Material Processing and Die and Mould Technology, Huazhong university of Science and Technology, Wuhan 4.0074. Hubei, China 3. Wuhan Zhike Abrasive-Resistant Material Science and Technology Development Co Ltd, Wuhan 4.0073, Hubei, China 4. College of Science, Wuhan university of Technology, Wuhan 4.0079, Hubei, China) [a] School of Mechanical Engineering and Automation Wuhan Textile University Wuhan 430073 Hubei China [b] State Key Laboratory of Material Processing and Die and Mould Technology Huazhong University of Science and Technology Wuhan 430074 Hubei China [c] Wuhan Zhike Abrasive-Resistant Material Science and Technology Development Co Ltd Wuhan 430073 Hubei China [d] College of Science Wuhan University of Technology Wuhan 430079 Hubei China

Impact, friction and corrosion from the grinding balls and the grinding medium during the mineral processing result in liner breakage. Liner, made from Hadfield steel or alloyed steel, could not have served in wet grinding environment for more than ten months. Composite liner, made from HCWCI (high Cr white cast iron) and carbon steel, has been developed successfully with liquid-liquid composing process based on LFC (lost foam casting). The microstructure of composite was analyzed with optical microscope, SEM (scanning electron microscope)/EDX energy-dispersive X-ray and XRD (X-ray diffraction). According to micrograph, the combination region of two metals was staggered like dogtooth, no mixtures occurred between two liquid metals, and its interface presented excellent metallurgical bonding state. The results of mechanical property test show that, the hardness of HRC, the fracture toughness, and the bending strength are more than 61, 16.5 J/cm2.and 1 600 MPa, respectively. Comparison between liners made from bimetal composite and alloyed steel has also been investigated in industrial hematite ball mill. The results of eight months test in wet grinding environment prove that the service life of bimetal composite liner is three times as long as that of one made from alloyed steel.

关键词： composite liner bimetal liquid-liquid compound composite interface lost foam casting high Cr white cast iron

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Combination of drainage, water supply and environmental protection as well as rational distribution of water resource in Zhengzhou mining district

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Science China Earth Sciences 2005年第10期48卷 1768-1779页

作者： WU Qiang1, LI Duo1,2. DI Zhiqiang3, MIAO Ying3, ZHAO Suqi4.& GUO Qiwen5 1. Resource Exploitation Engineering College, CUMT, Beijing 100083. China 2. Shijiazhuang Engineering College, university of Economics, Shijiazhuang 050031, China 3. Shenyang Institute of Geology and Mineral Resources, Shenyang 110032. China 4. State Adminstration of Coal Mine Safety, Beijing 100013, China 5. Zhengzhou Coal Mine Company (Group), Zhengzhou 4.2.71, China Resource Exploitation Engineering College CUMT Beijing China Shijiazhuang Engineering College university of Economics Shijiazhuang China Shenyang Institute of Geology and Mineral Resources Shenyang China State Adminstration of Coal Mine Safety Beijing China Zhengzhou Coal Mine Company (Group) Zhengzhou China

The geological condition of coalfield is much complex in China. With increasing in mining depth and drainage amount, the contradiction of drainage, water supply and environ-mental protection is becoming more and more serious. However, the contradiction can be solved by the scientific management of optimizing combination of drainage, water supply and environ-mental protection. The Philip multiple objectives simplex method used in this article has searched for a possible solution at the first step, and then it goes on searching to find out whether there is a weight number that can lead the solution to the biggest. It can reduce the randomness and diffi-culty of traditional weight method which determine the weight number artificially. Some beneficial coefficients are vague and the number is larger in the model of water resource dispatch. So the vague layer analysis method can consider these vague factors fully, combining the qualitative and quantitative analysis together. Especially, this method can quantify the experiential judge-ment of policy decider, and it will turn to be more suitable if the structure of objective factors is complex or the necessary data are absent. In the paper, the two methods above are used to solve the plans of drainage, water supply and optimizing distribution of water resource in the Zhengzhou mining district.

关键词： combination of drainage, water supply and environmental protection, Philip multiple objective simplex method, vague layer analysis method, distribution of water resource.

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Gas formation mechanism of marine carbonate source rocks in China

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Science China Earth Sciences 2005年第4期48卷 441-453页

作者： ZHAO Wenzhi1, WANG Zhaoyun1, HE Haiqing2. ZHANG Mingjie3, WANG Hongjun1, WANG Yunpeng4.& QIN Yong5 1. Research Institute of Petroleum Exploration & Development, PetroChina, Beijing 100083. China 2. PetroChina Exploration & Production, Beijing 100011, China 3. Department of Geology, Lanzhou university, Lanzhou 730000, China 4. Guangzhou Geochemical Institute, Chinese Academy of Sciences, Guangzhou 51064., China 5. China university of Mining and Technology, Xuzhou 2.1000, China 1. Research Institute of Petroleum Exploration & Development 100083 PetroChinaBeijin China 2. PetroChina Exploration & Production 100011 Beijing China 3. Department of Geology Lanzhou University 730000 Lanzhou China 4. Guangzhou Geochemical Institute Chinese Academy of Sciences 510640 Guangzhou China 5. China university of Mining and Technology 221000 Xuzhou China

By breaking through the conventional ideology on the study of gas-formation mechanism of source rocks which focused on merely the characteristics of source rocks them- selves, and based on the development and distribution characteristics of marine carbonate source rocks in the medium-to-bottom parts of the Chinese superimposed sedimentary basins as well as various processes in the course of gas generation and reservoir forming, the complex hydrocarbon-generating model of carbonates is established. Such a model concerns not only the “three-stage” gas formation characteristics of carbonates, but also the gas generation process due to a thermal cracking of oil and the re-generation process of gas from heated secondary organic matters during the gas-generation and reservoir-forming course. The high-quality hy- drocarbon generating matter of marine carbonate source rocks determined a high gas-oil ratio and tended to form paleo-oil-reservoirs, representing an enrichment process of organic matters. The thermal cracking of oil in palaeo-oil-reservoirs is an important means for the effective forma- tion of gas reservoirs. The secondary organic matters in carbonate reservoirs may regenerate gas after a secondary deep burial, thus becoming an effective gas source.

关键词： carbonate, three-stage hydrocarbon generation, inhibitive effect of maturity, oil-cracking gas, second-ary asphalt gas.

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On the new results of global attractive set and positive invariant set of the Lorenz chaotic system and the applications to chaos control and synchronization

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Science in China(Series F) 2005年第3期48卷 304-321页

作者： LIAO Xiaoxin 1, 2. 3 , FU Yuli 4.& XIE Shengli 4.1. Department of Control Science & Control Engineering, Huazhong university of Science & Technology, Wuhan 4.0074. China 2. School of Automation, Wuhan university of Science & Technology, Wuhan 4.0070, China 3. School of Information, Central South university of Economy, Politics and Law, Wuhan 4.0064. China 4. School of Electronics & Information Engineering, South China university of Technology, Guangzhou 51064., China Correspondence should be addressed to Liao Xiaoxin (email: xiaoxin_liao@***) 1. Department of Control Science & Control Engineering Huazhong University of Science & Technology 430074 Wuhan China 2. School of Automation Wuhan University of Science & Technology 430070 Wuhan China 3. School of Information Central South University of Economy Politics and Law 430064 Wuhan China 4. School of Electronics & Information Engineering South China University of Technology 510640 Guangzhou China

Constructing a family of generalized Lyapunov functions, a new method is proposed to obtain new global attractive set and positive invariant set of the Lorenz chaotic system. The method we proposed greatly simplifies the complex proofs of the two famous estimations presented by the Russian scholar Leonov. Our uniform formula can derive a series of the new estimations. Employing the idea of intersection in set theory, we extract a new Leonov formula-like estimation from the family of the estimations. With our method and the new estimation, one can confirm that there are no equilibrium, periodic solutions, almost periodic motions, wandering motions or other chaotic attractors outside the global attractive set. The Lorenz butterfly-like singular attractors are located in the global attractive set only. This result is applied to the chaos control and chaos synchronization. Some feedback control laws are obtained to guarantee that all the trajectories of the Lorenz systems track a periodic solution, or globally stabilize an unstable (or locally stable but not globally asymptotically stable) equilibrium. Further, some new global exponential chaos synchronization results are presented. Our new method and the new results are expected to be applied in real secure communication systems.

关键词： Lorenz chaotic system global attractive set positive invariant set globally exponential tracking globally exponential synchronization.

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