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Effects of abnormally high heat stress on petroleum in reservoir——An example from the Tazhong 18 Well in the Tarim Basin

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Science china Earth Sciences 2008年第4期51卷 515-527页

作者： ZHU DongYa1, JIN ZhiJun1, HU WenXuan2 & ZHANG XueFeng3 1 petroleum exploration and Production institute, china petroleum & Chemical Corporation, beijing 100083, china 2 Department of Earth Sciences, Nanjing University, Nanjing 210093, china 3 School of Resource and Information, china University of petroleum, beijing 102249, china petroleum exploration and Production institute China Petroleum & Chemical Corporation Beijing China Department of Earth Sciences Nanjing University Nanjing China School of Resource and Information China University of Petroleum Beijing China

An igneous intrusion of 94m thick was discovered intruding into the Silurian sandstone from Tazhong 18 Well. The petroleum previously preserved in the Silurian sandstone reservoir was altered into black carbonaceous bitumen by abnormally high heat stress induced by the igneous intrusion. The reflec-tance of the carbonaceous bitumen reaches as high as 3.54%, indicating that the bitumen had evolved into a high thermal evolution level. Similar to the Silurian samples from the neighboring Tazhong 11, Tazhong 12, Tazhong 45 and Tazhong 47 wells, the distribution of C27, C28 and C29 steranes of the car-bonaceous bitumen is still "V" -shaped and can still be employed as an efficient parameter in oil source correlation. The "V" -shaped distribution indicates that the hydrocarbons from the Tazhong 18 and the neighboring wells were all generated from the Middle-Upper Ordovician hydrocarbon source rocks. However, the oil source correlation parameters associated with and terpanes had been changed greatly by the high heat stress and can no longer be used in oil source correlation. The δ 13C values of the pe-troleum from the neighboring wells are between -32.53‰ and -33.37‰, coincident with those of the Paleozoic marine petroleum in the Tarim Basin. However, the δ 13C values of the carbonaceous bitumen from the Tazhong 18 Well are between -27.18‰ and -29.26‰, isotopically much heavier than the pe-troleum from the neighboring wells. The content of light hydrocarbons (nC14-nC20) of the saturated hydrocarbon fraction in the carbonaceous bitumen is extremely higher than the content of heavy hy-drocarbons. The light/heavy hydrocarbon ratios (ΣnC21-/ΣnC22+) are between 4.56 and 39.17. In the saturated fraction, the even numbered hydrocarbons are predominant to the odd numbered, and the OEP (Odd to Even Predominance) values are between 0.22 and 0.49. However, the content of light hy-drocarbons in the petroleum from the neighboring wells is relatively low and the content of the even numb

关键词： Tarim Basin igneous intrusive abnormally high heat stress bitumen carbon isotope PAH

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Seismic wave propagating in Kelvin-Voigt homogeneous visco-elastic media

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Science china Earth Sciences 2006年第2期49卷 147-153页

作者： YUAN Chunfang1, PENG Suping1, ZHANG Zhongjie2 & LIU Zhenkuan3 1. china University of Mining & Technology, beijing 100083, china 2. institute of Geophysics, Chinese Academy of Sciences, beijing 100101, china 3. exploration and development research institute of Daqing Oilfield, Daqing 163712, china 1. china University of Mining & Technology Beijing 100083 China 2. institute of Geophysics Chinese Academy of Sciences Beijing 100101 China 3. exploration and development research institute of Daqing Oilfield Daqing 163712 China

This paper studies, under a small disturbance, the responses of seismic transient wave in the visco-elastic media and the analytic solution of the corresponding third-order partial differential equation. A plane wave solution of Kelvin-Voigt homogeneous visco-elastic third-order partial differ-ential equation with a pulse source is obtained. By the principle of pulse stacking of particle vibration, the result is extended to the solution of Kelvin-Voigt homogeneous visco-elastic third-order partial differential equation with any source. The velocities of seismic wave propagating and the attenuation of seismic wave in Kelvin-Voigt homogeneous visco-elastic media are discussed. The velocities of seismic wave propagating and the coefficient of attenuation of seismic wave in Kelvin-Voigt homogeneous visco-elastic media are derived, expressed as functions of density of the media, elastic modulus and visco-elastic coefficient. These results can be applied in inversing lithology parameters in geophysical prospecting.

关键词： Kelvin-Voigt visco-elastic velocity attenuation seismic wave.

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Carbon and hydrogen isotopic characteristics of natural gases from the Luliang and Baoshan basins in Yunnan Province, china

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Science china Earth Sciences 2006年第9期49卷 938-946页

作者： XU Yongchang1, LIU Wenhui2, SHEN Ping1, WANG Wanchun1, WANG Xiaofeng1, Tenger1, YAN Yaomin3 & LIU Ruobin3 1. Lanzhou Center of Oil & Gas Resources, institute of Geology and Geophsics, Chinese Academy of Sciences, Lanzhou 730000, china 2. research institute of petroleum exploration and Production, SINOPEC, beijing 100083, china 3. South Branch of petroleum exploration and Production Company, SINOPEC, Kuming 650000, china 1. Lanzhou Center of Oil & Gas Resources Institute of Geology and Geophsics Chinese Academy of Sciences Lanzhou 730000 China 2. research institute of petroleum exploration and Production SINOPEC Beijing 100083 China 3. South Branch of petroleum exploration and Production Company SINOPEC Kuming 650000 China

The Luliang and Baoshan basins of Yunnan Province are two small-sizedcontinental oil/gas-bearing sedimentary basins, which were developed at the bases of theCarboniferous and Devonian systems during the Late Tertiary, covering an area of 325 km^2 and 254km^2, respectively. Since the 1990s, there have been discovered small-sized natural gas pools inthese two basins. The natural gases are composed mainly of hydrocarbon gases, with nonhydrocarbonsaccounting for less than 2%. Of the hydrocarbon gases, methane accounts for more than 99%, and thecomponents above C_2 account for less than 0.2%. On the basis of previous studies of geologicalbackground, the composition of natural gases and their carbon isotopic composition, it has beendefined that these two gas pools are of bacterial origin. In this work we have comprehensivelymeasured the carbon and hydrogen isotopic composition of natural gases from these two basins andhave gone into the details of the mechanism of gas generation. The δ^(13)C_1 values of naturalgases from the Luliang Basin are within the range of -72.1 per thousand - -73.3 per thousand, andthe δD_(CH_4) values, -242 per thousand - -234 per thousand, indicating that the bacterial gasgeneration is dominated by the way of CO_2 reduction. It has been evidenced that undercontinental-facies fresh water conditions there did occur the CO_2 reduction as a process ofbacterial gas generation. The δ^(13)C_1 values of natural gases from the Baoshan Basin are withinthe range of - 62.5 per thousand - -63.5 per thousand, and the δD_(CH_4) values, -252 per thousand- -260 per thousand. These isotopic characteristics are fallen into transitional phase of acetatefermentation and CO_2 reduction as defined by Whiticar et al. (1986). An important discovery in theLuliang Basin is the carbon isotopic composition of ethane of purely biogenetic origin, i.e., itsδ^(13)C_2 values are within the range of - 61.2 per thousand - - 66.0 per thousand. These carbonisotopic values have been r

关键词： bacterial gas, carbon and hydrogen isotope, CO2 reduction, acetate fermentation.

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Gas formation mechanism of marine carbonate source rocks in china

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Science china Earth Sciences 2005年第4期48卷 441-453页

作者： ZHAO Wenzhi1, WANG Zhaoyun1, HE Haiqing2, ZHANG Mingjie3, WANG Hongjun1, WANG Yunpeng4 & QIN Yong5 1. research institute of petroleum exploration & development, petrochina, beijing 100083, china 2. petrochina exploration & Production, beijing 100011, china 3. Department of Geology, Lanzhou University, Lanzhou 730000, china 4. Guangzhou Geochemical institute, Chinese Academy of Sciences, Guangzhou 510640, china 5. china University of Mining and Technology, Xuzhou 221000, china 1. research institute of petroleum exploration & development 100083 PetroChinaBeijin China 2. petrochina exploration & Production 100011 Beijing China 3. Department of Geology Lanzhou University 730000 Lanzhou China 4. Guangzhou Geochemical institute Chinese Academy of Sciences 510640 Guangzhou China 5. china University of Mining and Technology 221000 Xuzhou China

By breaking through the conventional ideology on the study of gas-formation mechanism of source rocks which focused on merely the characteristics of source rocks them- selves, and based on the development and distribution characteristics of marine carbonate source rocks in the medium-to-bottom parts of the Chinese superimposed sedimentary basins as well as various processes in the course of gas generation and reservoir forming, the complex hydrocarbon-generating model of carbonates is established. Such a model concerns not only the “three-stage” gas formation characteristics of carbonates, but also the gas generation process due to a thermal cracking of oil and the re-generation process of gas from heated secondary organic matters during the gas-generation and reservoir-forming course. The high-quality hy- drocarbon generating matter of marine carbonate source rocks determined a high gas-oil ratio and tended to form paleo-oil-reservoirs, representing an enrichment process of organic matters. The thermal cracking of oil in palaeo-oil-reservoirs is an important means for the effective forma- tion of gas reservoirs. The secondary organic matters in carbonate reservoirs may regenerate gas after a secondary deep burial, thus becoming an effective gas source.

关键词： carbonate, three-stage hydrocarbon generation, inhibitive effect of maturity, oil-cracking gas, second-ary asphalt gas.

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Classification of carbonate gas condensate reservoirs using well test and production data analyses

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petroleum Science 2011年第1期8卷 70-78页

作者： Li Yong Li Baozhu Hu Yongle Xia Jing Liu Zhaowei Deng Xingliang She Zhicheng Fan Kun research institute of petroleum exploration and development PetroChinaBeijing 100083.China china National Oil ＆ Gas exploration and development Corporation PetroChinaBeijing 100034China Tarim Oilfield Company PetroChinaKorlaXingjiang 841000China

Carbonate reservoir patterns play an important role in the production performance of oil and gas wells,and it is usually classified through static data analysis which cannot reflect the actual well *** paper takes the Tazhong No.1 gas field in the Tarim Basin,china as an example to investigate the classification of carbonate *** classification method mainly combines well test analysis with production analysis—especially the Blasingame type curve *** on the characteristics of type curves for well test analysis and the Blasingame method,the relationship between the type curves and reservoir pattern was *** than 20 wells were analyzed and the reservoirs were classified into 3 major patterns with 7 ***,the classification results were validated by dynamic performance analysis of wells in the Tazhong No.1 gas *** the basis of the classification results,well stimulation（*** flooding in a single well） was carried out in three volatile-oil wells,and the oil recovery increased by up to 20%.

关键词： Carbonate reservoir pattern well test analysis production analysis type curve

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Control of neotectonic movement on hydrocarbon accumulation in the Kuqa Foreland Basin,west china

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petroleum Science 2010年第1期7卷 49-58页

作者： Jiang Zhenxue Li Lianxia Song Yan Tian Fenghua Zhao Mengjun Wang Haijiang Zhao Zhenxing State Key Laboratory of petroleum Resources and Prospecting China University of Petroleum Beijing 102249 China Basin and Reservoir research Center China University of Petroleum Beijing 102249 China exploration and development research institute PetroChina Beijing 100083 China Department of exploration ＆ development PetroChina CBM Limited Company Beijing 100013 China exploration Department Tarim Oilfield Company PetroChina Kuerle Xinjiang 841000 China No.8 Oil Production Plant Changqing Oilfield Company PetroChina Xi＇an Shaanxi 710018 China

Neotectonic movement refers to the tectonic movement that has happened since the Cenozoic, which is the latest movement. It has the most important influence on the basins in west china, especially on the hydrocarbon accumulation in the western foreland basins. We determined the time of neotectonic movement in the Kuqa Foreland Basin, which began from the Neogene, and analyzed the patterns of movement, which were continuous and fast subsidence in the vertical direction and intense lateral compression. The structure styles are that the faulting is weakened and the folding is strengthened gradually from north to south. We studied the control of neotectonic movement on the hydrocarbon accumulation process and model in the Kuqa Foreland Basin with basin simulation technique. The largest subsidence rate of the Kuqa Foreland Basin reached 1,200 m/Ma during the neotectonic movement, leading to rapid maturing of source rock within 5 Ma and a large quantity of hydrocarbon being generated and expelled. The thick neotectonic strata can form high quality reservoirs with the proved gas and oil reserves accounting for 5% and 27% of the total reserves, respectively. 86% of the structural traps were formed in the neotectonic movement period. The faults formed during the neotectonic movement serve as important migration pathways and they exist in the region where the hydrocarbon reservoirs are distributed. Abnormally high pressure caused by the intense lateral compression, thick neotectonic strata deposition and rapid hydrocarbon generation provide driving force for hydrocarbon migration. The accumulation elements match each other well over a short period, leading to many large gas fields formed later in the Kuqa Foreland Basin.

关键词： Kuqa Foreland Basin neotectonic movement accumulation element accumulation process accumulation model

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Distribution and State of Ni Contaminants on Resid Fluid Catalytic Cracking Catalysts—Characterization by AEM, EPMA, UV-Vis and TPR

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石油学报（石油加工） 1997年第S1期13卷 148-153页

作者： Xue Yongfang (research institute of petroleum Processing, beijing 100083) research institute of petroleum Processing Beijing 100083 China

ＤｉｓｔｒｉｂｕｔｉｏｎａｎｄＳｔａｔｅｏｆＮｉＣｏｎｔａｍｉｎａｎｔｓｏｎＲｅｓｉｄＦｌｕｉｄＣａｔａｌｙｔｉｃＣｒａｃｋｉｎｇＣａｔａｌｙｓｔｓ—ＣｈａｒａｃｔｅｒｉｚａｔｉｏｎｂｙＡＥＭ，ＥＰＭＡ，ＵＶＶｉｓ... 详细信息

ＤｉｓｔｒｉｂｕｔｉｏｎａｎｄＳｔａｔｅｏｆＮｉＣｏｎｔａｍｉｎａｎｔｓｏｎＲｅｓｉｄＦｌｕｉｄＣａｔａｌｙｔｉｃＣｒａｃｋｉｎｇＣａｔａｌｙｓｔｓ—ＣｈａｒａｃｔｅｒｉｚａｔｉｏｎｂｙＡＥＭ，ＥＰＭＡ，ＵＶＶｉｓａｎｄＴＰＲＸｕｅＹｏｎｇｆａｎｇ...

关键词： distribution state Ni contaminant equilibrium catalysts resid fluid catalytic cracking process

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The control of syndepositional faulting on the Eogene sedimentary basin fills of the Dongying and Zhanhua sags, Bohai Bay Basin

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Science china Earth Sciences 2004年第9期47卷 769-782页

作者： LIN Changsong1, ZHENG Herong2, REN Jianye1, LIU Jingyan1 & Qiu Yigang1 1. Department of Energy Geology, china University of Geosciences, beijing 100083, china 2. petroleum exploration and Production institute, Sino-petroleum and Chemistry Cooperation, beijing 100083, china china Univ Geosci Dept Energy Geol Beijing 100083 Peoples R China Sino Petr & Chem Cooperat Petr Explorat & Prod Inst Beijing 100083 Peoples R China

The Dongying and Zhanhua sags are the major hydrocarbon exploration and produc- tion subbasins in the Bohai Bay Basin. Integrated analysis of the sedimentary basin fills has shown that the syndepositional faults and their arrangement styles exerted an important influ- ence on the development and distribution of the Eogene depositional systems. The sedimentary filling evolution of the subbasins reflects the general control of the episodic rifting process. The major long-term active normal faults formed a series of paleogeomorphic accident or slopebreak zones that commonly delineated the subsidiary palaeostructural units and the depositional facies tracts and constrained the general distribution of sedimentary facies zones. The central sag boundary fault slopebreak zones usually determined the distribution of the depocenters of ter- restrial clastic depositional systems, particularly the lowstand fans or deltaic depositional sys- tems, and have proven to be the economically important targets for the exploration of subtle sandstone reservoirs. A variety of syndepositional fault arrangement patterns, including the par- allel, en echelon, combo-like, broom-like fault systems and the fault overlap or transfer zones, have been recognized in the subbasins. They generated distinctive geomorphic features and exerted a direct influence on sediment dispersal and sandbody distribution during the Eogene synrift stage. It is the key for the prediction of depositional systems tracts and reservoir sand- stones to investigate the activity and distribution of the fault slopebreak zones and reconstruct the structural paleogeomorphy in different basin filling stages of the basin evolution.

关键词： episodic rifting, fault slopebreak zone, depositional pattern, Bohai Bay Basin.

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SOME CHARACTERISTICS OF GAS POOLS (FIELDS) IN china

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石油勘探与开发 1997年第2期24卷 91-95页

作者： Dai Jinxing( Academician of the Chinese Academy of Sciences research Insitute of Petdsm exploration and development, CNPC, beijing, 100083)

Chinese natural gas Pools (fields) are chiefly hydrocarbon gas pools (fields), with a few of CO2 and a tiny of H2S ones. The gas genetic types are multiple, dominated by oil-type gas and coal-formed gas types,and then followed by other types such as the biogas, mixed gas, H2S-rich gas and abiogenetic gas etc.. The medium-large sized gas pools (fields), in number, account for onIy 13% of the total gas and oil-gas fields in china, but they pes more than 70% gas reserves of the total. The abiogenetic CO2 gas pooIs (fields) are mainly located in the eastern oil-gas bearing basins, such as the Bohai Bay, Songliao, Subei, Sanshui, East china Sea and Zhujiangkou basins etc.. Natural gas pools (fields) tend to develop in or surround the gas generation centers of sedimentary basins.

关键词： Natural gas Gas reservoir Gas field Feature Gas reservoir type Natural gas origin Petroliferous basin (Gas generation center)

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The controlling factors and distribution prediction of H2S formation in marine carbonate gas reservoir,china

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Science Bulletin 2007年第S1期 150-163页

作者： ZHU GuangYou, ZHANG ShuiChang & LIANG YingBo research institute of petroleum exploration and development, petrochina, beijing 100083, china

Generally, there are some anhydrites in carbonate reservoir, as H2S is also familiar in carbonate oil and gas reservoirs. Nowadays, natural gas with high H2S concentration is usually considered as TSR origin, so there is close relationship between H2S and anhydrite. On the contrary, some carbonate rocks with anhydrite do not contain H2S. Recently, researches show that H2S is only a necessary condition of H2S formation. The reservoir porosity, sulfate ion content within formation water, reservoir temperature, oil/gas and water interface, hydrocarbon and some elements of reservoir rock have great controlling effects on the TSR occurrence. TSR deoxidizes hydrocarbon into the acidic gas such as H2S and CO2, and the H2S formation is controlled by TSR occurrence, so the relationship among reaction room, the contact chance of sulfate ion and hydrocarbon, the reservoir temperature has great influence on the TSR reaction. H2S has relatively active chemical quality, so it is still controlled by the content of heavy metal ion. Good conditions of TSR reaction and H2S preservation are the prerequisite of H2S distribution prediction. This paper builds a predictive model based on the characteristic of natural gas reservoir with high H2S-bearing. In the porosity reservoir with anhydrite, the formation water is rich in sulfate and poor in heavy metal ion. Oil and gas fill and accumulate in the gas reservoir with good preservation conditions, and they suffered high temperature later, which indicates the profitable area of natural gas with high H2S-bearing.

关键词： H2S carbonate rock distribution prediction controlling factors TSR Sichuan Basin

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