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The components and carbon isotope of the gases in inclusions in reservoir layers of Upper Paleozoic gas pools in the Ordos Basin,china

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Science china Earth Sciences 2008年第S1期51卷 115-121页

作者： MI JingKui 1 ,DAI JinXing 1 ,ZHANG ShuiChang 1 ,ZHANG WenZheng 2 ,GONG Se 1 &LI XianQing 3.1 research institute of petroleum Exploration and {3.,petrochina,Beijing 100083.china 2 Exploration and {3. research institute of petrochina Changqing Oilfield Company,Xi’an 710021,china 3.Key Laboratory of Coal Resources,Ministry of Education,china University of Miningand Technology,Beijing 100083.china petrochina Res Inst Petr Explorat & Dev Beijing 100083 Peoples R China petrochina Changqing Oilfield Co Explorat & Dev Res Inst Xian 710021 Peoples R China china Univ Min & Technol Key Lab Coal Resources Minist Educ Beijing 100083 Peoples R China

The components and carbon isotope of gases in inclusions are one of the most important geochemical indexes for gas *** analysis results of the components and carbon isotope of gases from inclusions in reservoir layers of Upper Palaeozoic gas pools in the Ordos Basin show that most inclusions grown in reservoir sandstone are primary *** is only a little difference about the components and carbon isotope between the well gases and the secondary inclusions *** indicated that the epigenetic change of gas pools is *** difference between the well gases and the secondary inclusions gases is caused by two reasons:(i)The well gases come from several disconnected sand bodies buried in a segment of depth,while the inclusion gases come from a point of depth.(ii)The secondary inclusions trapped the gases generated in the former stage of source rock gas generation,and the well gases are the mixed gases generated in all the *** is irresponsible to reconstruct the palaeo-temperature and palaeo-pressure under which the gas pool formed using carbon dioxide inclusions.

关键词： Ordos Basin Upper Paleozoic inclusion gas components carbon isotope

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Identification of marine natural gases with different origin sources

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Science china Earth Sciences 2008年第S1期51卷 148-164页

作者： WANG YunPeng 1 ,ZHAO ChangYi 2 ,WANG ZhaoYun 2 ,WANG HongJun 2 ,TIAN Jin 1 ,ZOU YanRong 1 &LIU JinZhong1 1State Key Laboratory of Organic Geochemistry,Guangzhou institute of Geochemistry,Chinese Academy of Sciences,Guangzhou 510640,china 2institute of Geology,{3. institute of petroleum Exploration and development,petrochina,Beijing 100083.china State Key Laboratory of Organic Geochemistry Guangzhou Institute of Geochemistry Chinese Academy of Sciences Guangzhou 510640 China institute of Geology Research Institute of Petroleum Exploration and Development PetroChina Beijing 100083

Kinetic experiments of gas generation for typical samples of marine gas precursors including low-maturity kerogen,residual kerogen and oil as well as dispersed liquid hydrocarbon(DLH)in source rocks were performed by closed system,and the evolution trends of molecular and isotopic compositions of natural gases from different precursors against the maturity(R0%)at laboratory conditions were *** diagrams of gas origin were calibrated by using the experimental data.A diagram based on the ratio of normal and isomerous butane and pentane(i/nC4-i/nC5)was proposed and used to identify the origins of the typical marine natural gases in the Sichuan Basin and the Tarim Basin, *** the maturities of natural gases were estimated by using the statistical relationships between the gaseous molecular carbon isotopic data and maturities(δ13.-R 0 %)with different *** results indicate that the molecular and isotopic compositions of simulated gases from different precursors are different from each *** example,the dryness index of the oil-cracking gas is the lowest;the dryness indices of gases from DLH and kerogen in closed system are almost the same;and the dryness index of gases from residual kerogen is extremely high,indicating that the kerogen gases are very dry;the contents of non-hydrocarbon gases in kerogen-cracking gases are far higher than those in oil-cracking and DLH-cracking *** molecular carbon isotopes of oil-cracking gases are the lightest,those of kerogen in closed system and GLH-cracking gases are the second lightest,and those of cracking gases from residual kerogen are the *** calibration results indicate that the diagrams of ln(C1/C2)-ln(C2/C3.andδ13.2-δ13.3.ln(C2/C3.can discriminate primary and secondary cracking gases,but cannot be used to identify gas origin sources,while the diagram of i/nC4-i/nC5 can differentiate the gases from different *** application results of these diagrams show that gas mixtures ext

关键词： marine organic matter gas origin sources kerogen oil-cracking gas origin identification carbon isotope

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Cracking conditions of crude oil under different geological environments

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Science china Earth Sciences 2008年第S1期51卷 77-83页

作者： ZHAO WenZhi,WANG ZhaoYun,ZHANG ShuiChang&WANG HongJun research institute of petroleum Exploration&{3.,petrochina,Beijing 100083.china petrochina Res Inst Petr Explorat & Dev Beijing 100083 Peoples R China

There are mainly 3.kinds of existing states of oil generating from source rocks,that is,dispersive liquid hydrocarbon inside of source rock,dispersive liquid hydrocarbon outside of source rock and concentrated liquid hydrocarbon outside of source *** of the differences in thermal history and medium conditions around,and the interaction of organic and inorganic matter,the liquid hydrocarbon with 3.kinds of existing state has different cracking *** gas generation dynamics experiments of crude oil matching different mediums indicate that the distribution of activation energy of methane changes a lot according to medium *** carbonate has a main influence on oil cracking conditions and can largely reduce its activation energy,which reflects the lower cracking temperature of crude *** mudstone takes a second place and the sandstone is the *** catalytic cracking function to the oil of the carbonate,of the mudstone and of the sandstone changes weaken in *** corresponding Ro values of main gas generation period in different mediums are as follows:1.5%―3.8%with pure crude oil,1.2%―3.2%with dispersive crude oil in carbonate,1.3.~3.4% with dispersive crude oil in mudstone and 1.4%―3.6%with dispersive crude oil in *** influence of pressure to crude oil cracking is relatively *** the low heating speed condition, pressure restrains the oil cracking and gas generation,but in the high heating speed condition,pressure has an indistinctive influence to the oil cracking and gas *** also makes a different effort in different evolvement *** the middle and lower Cambrian source rocks in the Tarim Basin as an example,primary oil generating quantity is 223..24×10 8 t,residual oil and oil cracking gas quantity is 806.21×10 8 t and 106.95×10 12 m 3.respectively.

关键词： different existing state oil cracking condition gas source rock kitchen of oil cracking type

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Application of backflush and micro-flow techniques to the analysis of C5—C13.hydrocarbons in crude oils and its geochemical significance

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Progress in Natural Science:Materials International 2007年第11期17卷 1382-1387页

作者： Wang Peirong1,2, Zhao Hong2,3. Xu Guanjun1,4, Zhu Cuishan2,3. Xiao Tingrong4, Zhang Min2,3.and Zhang Bin1,4(1. Key Laboratory of petroleum Geochemistry, china National petroleum Corporation, Beijing 100083. china 2. Geochemistry Department of Yangtze University, Jingzhou 43.023. china 3. Key Laboratory of Exploration Technologies for Oil and Gas Resources, Ministry of Education, Yangtze University, Jingzhou 43.023. china 4. petroleum Geology Central Laboratory, research institute of petroleum Exploration and development, petrochina, Beijing 100083. china) Key Laboratory of petroleum Geochemistry China National Petroleum Corporation Beijing 100083 China Geochemistry Department of Yangtze University Jingzhou 434023 China Key Laboratory of Exploration Technologies for Oil and Gas Resources Ministry of Education Yangtze University Jingzhou 434023 China petroleum Geology Central Laboratory Research Institute of Petroleum Exploration and Development PetroChina Beijing 100083 China

An Agilent 6890N GC equipped with both FID and Agilent 5975 MSD analyzer has been employed to analyze C5—C13.hydrocarbon fractions of crude oils. A technical combination of program temperature volatilizer injection, backflush and micro-flow controller afforded a fine separation of C5—C13.compounds on a PONA column with the heavy part of crude oils being cut off before entering the analytical column. Both GC-FID chromatogram and GC-MS mass chromatograms (MID and full scan) could be obtained at the same time. The retension time differences of nC6—nC13.alkanes between GC and TIC were in the range of 0.02—0.58 minutes. Totally 286 peaks have been assigned group compositions. Results on 8 typical oil samples from CNPC Key Laboratory Crude Oil Library showed that the characteristics of C6—C13.hydrocarbon group composition could be used in oil-oil correlation studies.

关键词： GC analysis GC/MS analysis backflush micro-flow controller light fraction in crude oil

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Discovery of a Late Permian Angara-Cathaysia mixed flora from Acheng of Heilongjiang,china,with discussions on the closure of the Paleoasian Ocean

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Science china Earth Sciences 2009年第12期52卷 1746-1755页

作者： DENG ShengHui1,2, WAN ChuanBiao3.& YANG JianGuo3.1 research institute of petroleum Exploration and {3., petrochina, Beijing 100083. china 2 State Key Laboratory of Enhanced Oil Recovery, Beijing 100083.china 3.Daqing institute of petroleum Exploration and {3., petrochina, Daqing 164712, china research institute of petroleum Exploration and {3. PetroChina Beijing 100083 China State Key Laboratory of Enhanced Oil Recovery Beijing 100083 China Daqing institute of petroleum Exploration and development PetroChina Daqing 164712 China

This work documents a new flora from the Upper Permian Hongshan Formation of Acheng County, Heilongjiang Province, Northwest china. The flora consists of 20 species: Paracalamites sp., Pecopteris tangwangheensis Huang, Callipteris obese Huang, Callipteris shenshuensis Huang, C. tangwangheensis Huang, C. heilongjiangensis Huang, C. zeilleri Zalessky, C. sp., Comia yichunensis Huang, C. tenueaxis Huang, Iniopteris sibirica Zalessky, Supaia teiliensis Huang, Compsopteris tchirkovae Zalessky, C. cf. adzvensis Zalessky, Nilssonia sp. 1, Nil. sp. 2, Taeniopteris cf. densissima Halle, T. cf. nystraemii Halle, T. sp. and Noeggerathiopsis derzavinii Neub. It is dominated by Angara species but mixed with some typical Cathaysian elements. The age of the flora is assigned to late of the Late Permian according to the stratigraphic ranges of the known species and the comparisons of it with the similar floras. The new discovery indicates that the final collision between the North china Plate and Siberian Plate occurred in Late Permian along the Xar Moron River-Changchun-Yanji sutured zone, and the Paleoasian Ocean was finally closed at the end of the Permian.

关键词： Late Permian mixed Angara-Cathaysia flora Paleoasian Ocean plate collision Heilongjiang Province of china

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A method of identifying effective source rocks and its application in the Bozhong Depression,Bohai Sea,china

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petroleum Science 2010年第4期7卷 458-465页

作者： Jiang Fujie Pang Xiongqi Meng Qingyang Zhou Xiaohui Basin and Reservoir research Center China University of Petroleum Beijing 102249 China State Key Laboratory of petroleum Resource and Prospecting Beijing 102249 China research institute of petroleum Exploration and {3. PetroChina Beijing 100083 China

research on effective source rocks directly affects the accuracy of identifying hydrocarbon resources, and indirectly affects the exploration decisions in petroliferous basins. Although the previous evaluation methods of effective source rocks vary relatively widely, a complete quantitative evaluation approach has not yet been developed. For that reason, we redefined the concept of effective source rocks based on the existing research results. Surrounding this definition, and guided by the hydrocarbon expulsion theory, the quantitative model called ＂two stages and three steps＂ method is established to predict effective source rocks. Its application in the Bozhong Depression indicates that among the four sets source rocks in the Bozhong Depression, the Member 3.of the Shahejie Formation （Es 3.） has the largest effective source rock thickness, and the Member 1 Member 2 of the Shahejie Formation （Es 1＋2 ） is the second largest .The effective part of dark mudstone is only 3.%-80% of the total volume and with the increase of buried depth and improvement of quality, the effective part increases. Comprehensive analysis indicates that the ＂two stages and three steps＂ method is a practical technique for effective source rock prediction.

关键词： Source rock effectiveness hydrocarbon expulsion threshold Bozhong Depression Bohai Sea

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Evaluation criteria for gas source rocks of marine carbonate in china

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Progress in Natural Science:Materials International 2005年第9期15卷 810-817页

作者： WANG Zhaoyun1**, ZHAO Wenzhi1 and WANG Yunpeng2(1. research institute of petroleum Exploration & {3.,petrochina, Beijing 100083. china 2. Guangzhou institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, china) research institute of petroleum Exploration & {3. PetroChina Beijing 100083 China. Guangzhou institute of Geochemistry Chinese Academy of Sciences Guangzhou 510640 China

Hydrocarbon generating and expulsion simulation experiments are carried out using samples artifically matched between the acid-dissolved residue of relatively low-maturity limestone and the original sample. This work makes up for the insufficiency of source rock samples with high abundance of organic matters and low maturity in china. The organic carbon content of the 10 prepared samples varies between 0.15% and 0.74%. Pyrolysis data and simulation experiment results of hydrocarbon generating and expulsion, which were obtained by a high-temperature and high-pressure open system, indicate that the lower limit of organic carbon content for marine carbonate rock to generate and expel hydrocarbons is 0.23.—0.3.%. In combination with the numerical analysis of organic carbon in marine carbonate rocks from Tarim Basin, Sichuan Basin, Ordos Basin and North china, as well as the contribution of these gas source rocks to the discovered gas pools, we think that the organic carbon criterion for carbonate gas source rocks should be 0.3..

关键词： carbonate gas source rock gas-generating efficiency evaluation criteria simulation experiment.

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An analysis of seismic attenuation in random porous media

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Science china(Physics,Mechanics & Astronomy) 2010年第4期53卷 628-637页

作者： LIU Jiong1, BA Jing2, MA JianWei1 & YANG HuiZhu1 1 institute of Seismic Exploration, School of Aerospace, Tsinghua University, Beijing 100084, china 2 research institute of petroleum Exploration & development, petrochina, Beijing 100083. china 1. institute of Seismic Exploration School of Aerospace Tsinghua University Beijing 100084 China2. Research Institute of Petroleum Exploration & Development PetroChina Beijing 100083 China

The attenuation of seismic wave in rocks has been one of the interesting research topics, but till now no poroelasticity models can thoroughly explain the strong attenuation of wave in rocks. In this paper, a random porous medium model is designed to study the law of wave propagation in complex rocks based on the theory of Biot poroelasticity and the general theory of stochastic process. This model sets the density of grain, porosity, permeability and modulus of frame as random parameters in space, and only one fluid infiltrates in rocks for the sake of better simulation effect in line with real rocks in earth strata. Numerical simulations are implemented. Two different inverse quality factors of fast P-wave are obtained by different methods to assess attenuation through records of virtual detectors in wave field (One is amplitude decay method in time domain and the other is spectral ratio method in frequency domain). Comparing the attenuation results of random porous medium with those of homogeneous porous medium, we conclude that the attenuation of seismic wave of homogeneous porous medium is far weaker than that of random porous medium. In random porous media, the higher heterogeneous level is, the stronger the attenuation becomes, and when heterogeneity σ = 0.15 in simulation, the attenuation result is consistent with that by actual observation. Since the central frequency (50 Hz) of source in numerical simulation is in earthquake band, the numerical results prove that heterogeneous porous structure is one of the important factors causing strong attenuation in real stratum at intermediate and low frequency.

关键词： the theory of stochastic process the theory of Biot poroelasticity the attenuation of seismic wave inverse quality factor

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Characteristics of hydrocarbon sources and controlling factors of their formation in Pingliang Formation,West Ordos Basin

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Science Bulletin 2007年第S1期 103-112页

作者： CHEN MengJin1, NING Ning2, HU GuoYi2 & LI Jian2 1 Ordos branch of research institute of {3. Exploration and development, petrochina, Beijing 100083. china 2 langfang branch of research institute of {3. Exploration and development, petrochina, langfang 065007, china

According to organic geochemistry and organic petrology, the hydrocarbon sources in Pingliang Formation, W. Ordos basin, are systematically evaluated. The organic abundance of hydrocarbon source in this research is higher in the upper part of profiles than in the low, and more in mudstone than in carbonate. Most of organic matters become sapropelic, and few are humic-sapropelic in the regions of Shibangou and Zhuzisan. According to stable isotopes of carbon and oxygen in carbonate rock, boron index and ratios of elements, palaeo-salinity and sedimentary velocity are calculated. The two factors of paleao-salinity and sediment velocity, which control the distribution of organic matters, are discussed. Good relationship is found between water salinity and abundance of organic matter; in contrast, poor correlation is observed between salinity and types of organic matters. The relative sediment velocity in the research regions is also related with organic abundance and types. A low sediment velocity would lead to high abundance and good type of organic matters, and vice versa.

关键词： Ordos Basin Pingliang Formation abundance kerogen type palaeo-salinity sedimentary velocity

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A hydrocarbon enrichment model and prediction of favorable accumulation areas in complicated superimposed basins in china

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petroleum Science 2010年第1期7卷 10-19页

作者： Pang Xiongqi Meng Qingyang Jiang Zhenxue Liu Luofu Lu Xiuxiang State Key Laboratory of petroleum Resources and Prospecting China University of Petroleum Beijing 102249 China Basin and Reservoir research Center China University of Petroleum Beijing 102249 China research institute of petroleum Exploration and {3. PetroChina Beijing 100083 China

The geologic conditions of superimposed basins in china are very complicated. This is mainly shown by multi-phase structural evolution, multiple sets of source-reservoir-cap rock combinations, multiple stages of hydrocarbon generation and expulsion from source rocks, multi-cycle hydrocarbon enrichment and accumulation, and multi-phase reservoir adjustment and reconstruction. The enrichment, accumulation and distribution of hydrocarbon is mainly controlled by the source rock kitchen, paleo- anticline, regional cap rock and intensity of tectonic movement. In this paper, the T-BCMS model has been developed to predict favorable areas of hydrocarbon accumulation in complicated superimposed basins according to time and spatial relationships among five key factors. The five factors include unconformity surface representing tectonic balancing （B）, regional cap rock representing hydrocarbon protection （C）, paleo-anticline representing hydrocarbon migration and accumulation （M）, source rock kitchen representing hydrocarbon generation and expulsion （S） and geological time （T）. There are three necessary conditions to form favorable areas of hydrocarbon accumulation. First, four key factors BCMS should be strictly in the order of BCMS from top to bottom. Second, superimposition of four key factors BCMS in the same area is the most favorable for hydrocarbon accumulation. Third, vertically ordered combination and superimposition in the same area of BCMS should occur at the same geological time. The model has been used to predict the most favorable exploration areas in Ordovician in the Tarim Basin in the main hydrocarbon accumulation periods. The result shows that 95% of the discovered Ordovician hydrocarbon reservoirs are located in the predicted areas, which indicates the feasibility and reliability of the key factor matching T-BCMS model for hydrocarbon accumulation and enrichment.

关键词： Complicated superimposed basin key factor matching T-BCMS model favorable area for hydrocarbon accumulation hydrocarbon distribution prediction

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