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Surface Nanocrystallization of Magnesium Alloy AZ91D by High-Energy Shot Peening

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Journal of Wuhan university of technology(materials {3.) 2009年第4期24卷 515-519页

作者：张津 School of materials science & engineering University of Science and Technology Beijing college of materials science & {3. Chongqing University of Technology

High-energy shot peening （HESP）, a method to produce severe plastic deformation by high velocity flying balls, was applied on die cast magnesium alloy AZ91D. Effects of surface nanocrystallization by HESP and heat treatment at different temperatures were investigated. The mi- crostructure evolution was conducted using X-ray diffraction （XRD） and field emission scanning electronic microscopy （FESEM）. The hardness was measured by microhardness tester. The experimental results show that surface nanocrystrallization of AZ91D obtained by HESP would lead to the increase of microhardness. Low temperature heated at 100℃ for 1 h do not change the property obviously. However, both the microstructure and microhardness vary greatly after heat treatment at 400℃ for 1 h.

关键词： AZ91 D surface nanocrystallization HESP microhardnss corrosion resistance

Preparation of semi-solid AlSi7Mg alloy slurry with big capability

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Rare Metals 2010年第6期29卷 642-645页

作者： LI Sha and MAO Weimin School of materials science and engineering,{3. of science and technology Beijing,Beijing 100083.china School of materials science and engineering University of Science and Technology Beijing Beijing China

Semi-solid AlSi7Mg alloy slurry was prepared by low superheat pouring and weak traveling-wave electromagnetic *** effects of pouring temperature and stirring power on the microstructure of AlSi7Mg alloy slurry were *** results show that the semi-solid AlSi7Mg alloy slurry of 5 kg can be *** new technology can save energy and make the pouring process *** the pouring temperature is decreased at a stirring power of 0.41 kW,the shape of primary α-Al grains gradually changes from dendritic-like to *** the alloy melt is poured at the temperature（63.°C） with a certain superheat,the pouring process becomes easier,and the spherical microstructure of AlSi7Mg alloy slurry can be prepared by the weak traveling-wave electromagnetic *** the pouring temperature is 63.°C,increasing the stirring power appropriately can result in better spherical primary α-Al grains,but if the stirring power is increased to a certain value（1.72 kW）,the shape of primary α-Al grains does not obviously improve when the stirring power is continually increased.

关键词： aluminum alloys metal forming semisolid slurry electromagnetic stirring microstructure

Dislocation Densites of Deformed Steel Sheets Based on Positron Annihilation

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International Journal of Minerals,Metallurgy and materials 1998年第1期12卷 47-50页

作者： Yonglin Kang Xianjin Wang (materials science and engineering School,{3. Beijing, Beijing 100083. china) materials science and engineering School University of Science and Technology Beijing Beijing 100083 China

The variation regularity of dislocation densites of some deformed steel sheets under three kinds of strainpaths as uniaxial tension, plane strain and equal biaxial stretching was investigated by means of positron lifetimespectrum and Doppler-broadening techniques. The results show that the increasing rate of dislocation densites isrelated to the plastic strain path. A relationship between the increasing rate of micro-defects, macro-instability andforming limits during the process of steel sheet forming was got based on analyzing the mechanism of dislocationdensity increasing under different stress-strain condihons.

关键词： positron annihilation dislocation steel sheet strain path

Sol-gel Preparation and Infrared Radiation Property of Boron-substituted Cordierite Glass-ceramics

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Journal of materials science & technology 2010年第5期26卷 445-448页

作者： Shuming Wang and Fenghua Kuang School of materials science and engineering,{3. of science & technology Beijing,Beijing 100083.china [a] School of materials science and engineering university of science & technology Beijing Beijing 100083 china

Boron for aluminum substitution in the cordierite structure has been examined by sol-gel preparation of different samples along the compositional junction Mg2Al4-xBxSi5O18 with x=0,0.5,1,*** increasing the x value from 0 to 1.5 the crystallization behavior changed *** amount B2O3.doping can promote the sintering of amorphous cordierite gel,effectively restrain the precipitation of μ-cordierite and enhance the crystallization of α-*** substitution of B3. for Al3. in cordierite crystal structure can effectively improve the near-infrared spectral emissivity of this cordierite based glass-ceramics.

关键词： Sol-gel Glass-ceramics Infrared radiation B3. substitution Solid solution

Effects of silver powder particle size on the microstructure and properties of Ag-Yb_2O_3.electrical contact materials prepared by spark plasma sintering

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Rare Metals 2010年第4期29卷 366-370页

作者： CHEN Xiaohua,JIA Chengchang,and LIU Xiangbing School of materials science and engineering,{3. of science and technology Beijing,Beijing 100083.china School of materials science and engineering University of Science and Technology Beijing Beijing China

mg-Yb203.electrical contact materials were fabricated by spark plasma sintefing （SPS）. The effects of silver powder particle size on the microstructure and properties of the samples were investigated. The surface morphologies of the sintered samples were examined by optical microscope （OM）, and the fracture morphologies were observed by scanning electron microscopy （SEM）. The physical and mechanical properties such as density, electrical resistivity, microhardness, and tensile strength were also tested. The results show that the silver powder particle size has evident effects on the sintered materials. Comparing with coarse silver powder （5 ktm）, homogeneous and fme microstmcture was obtained by fine silver powder （_〈0.5-1am）. At the same time, the electrical conductivity, microhardness, and tensile strength of the sin- tered samples with fine silver powder were higher than those of the samples with coarse silver powder. However, silver powder particle size has little influence on the relative densities, which of all samples （both by free and coarse silver powders） is more than 95%. The fracture characteristics are ductile.

关键词： composites electrical contact materials spark plasma sintering particle size microstructure physical properties mechanical properties

Analysis on Microstructure and Misorientation of Ultrathin Hot Strip of Low Carbon Steel Produced by Compact Strip Production

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Journal of materials science & technology 2002年第6期18卷 501-503页

作者： Hao YU, Yonglin KANG and Jie FUSchool of materials science and engineering,{3. Beijing, Beijing 100083. china Sch. of Mat. Sci. and Eng. Univ. of Sci. and Technol. Beijing Beijing 100083 China

The microstructure and misorientation of ultrathin hot strip were analyzed by CSP technology using electron back scattered diffraction (EBSD) method and Autoforge finite element program. The experimental results showed that the finishing hot rolling microstructures were the mixture of recrystallized and deformed austenite. After phase transformation, ferrite grains embody substructures and dislocations, leading to the high strength and relatively low elongation rate of the ultrathin hot strip. The FEM simulation of strain mode and distribution in deformation area has been fulfilled. The simulation results are in good agreement with the theoretical analysis and experimental results.

关键词： CSP Electron back scattered diffraction, Texture, Finite element method

Microstructural Features During Strain Induced Ferrite Transformation in 08 and 20Mn Steels

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Journal of university of science and technology Beijing 2001年第2期8卷 105-110页

作者： Ping Yang, Feng-e Cui, Fuming Wang (materials science and engineering School,{3. Beijing, Beijing 100083. china) (Metallurgy School,{3. Beijing, Beijing 100083. china) Univ Sci & Technol Beijing Mat Sci & Engn Sch Beijing 100083 Peoples R China Univ Sci & Technol Beijing Met Sch Beijing 100083 Peoples R China

The microstructure evolution during strain induced ferrite transformation was followed in thermal-simulation tests of clean 08 and 20Mn steels. The influences of carbon equivalence and initial austenite grain size on ferrite grain refinement and the volume fraction of ferrite during straining were inspected. The results revealed that the accelerating effect of ferrite transformation by strain was increased as the carbon equivalence decreased. However, finer ferrite grains were obtained at higher carbon content. At strain of similar to1.5 ferrite grains less than 3.mum and 2 mum can be obtained in 08 and 20Mn steels respectively. Whereas the ferrite grain refinement in 08 steel was due to both effects of strain induced transformation and ferrite dynamic recrystallization, that in 20Mn was mainly due to strain induced transformation. Heavy strain can produce fine ferrite grains in coarse austenite grained 08 steel, but it would lead to band microstructure in coarse austenite grained 20Mn.

关键词： clean carbon steel strain induced transformation grain refinement ferrite dynamic recrystallization

Optimization of thermomechanical processes in Cu-Cr-Zr lead frame alloy using neural networks and genetic algorithms

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science china(Technological sciences) 2005年第5期48卷 510-520页

作者： SU Juanhua1,2, LIU Ping2, DONG Qiming2 & LI Hejun1 1. college of materials science and {3., Northwestern Polytechnical university, Xi’an 710072, china 2. college of materials science and {3., Henan university of science and technology, Luoyang 471003. china 1. college of materials science and {3. Northwestern Polytechnical University 710072 Xi’an China 2. college of materials science and {3. Henan University of Science and Technology 471003 Luoyang China

The thermomechanical treatment process is effective in enhancing the properties of the lead frame copper alloy. In this study, an optimal pattern of the thermomechanical processes for Cu-Cr-Zr was investegated using an intelligent control technique consisting of neural networks and genetic algorithms. The input parameters of the artificial neural network (ANN) are the reduction ratio of cold rolling, aging temperature and aging time. The outputs of the ANN model are the two most important properties of hardness and conductivity. Based on the successfully trained ANN model, genetic algorithms (GA) are used to optimize the input parameters of the model and select perfect combinations of thermomechanical processing parameters and properties. The good generalization performance and optimized results of the integrated model are achieved.

关键词： Cu-Cr-Zr alloy, thermomechanical processing optimization, artificial neural network, genetic algorithms.

Effect of powder mixing process on the microstructure and thermal conductivity of Al/diamond composites fabricated by spark plasma sintering

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Rare Metals 2010年第1期29卷 86-91页

作者： CHU Ke, JIA Chengchang, LIANG Xuebing, and CHEN Hui School of materials science and engineering,{3. Beijing, Beijing 100083. china School of materials science and engineering University of Science and Technology Beijing

Two powder mixing processes, mechanical mixing （MM） and mechanical alloying （MA）, were used to prepare mixed Al/diamond powders, which were subsequently consolidated using spark plasma sintering （SPS） to produce bulk Al/diamond composites. The effects of the powder mixing process on the morphologies of the mixed powders, the microstructure and the thermal conductivity of the composites were investigated. The results show that the powder mixing process can significantly affect the microstructure and the thermal conductivity of the composites. Agglomerations of the particles occurred in mixed powders using MM for 3. min, which led to high pore content and weak interfacial bonding in the composites and resulted in low relative density and low thermal conductivity for the composites. Mixed powders of homogeneous distribution of diamond particles could be obtained using MA for 10 min and MM for 2 h. The composite prepared through MA indicated a high relative density but low thermal conductivity due to its defects, such as damaged particles, Fe impurity, and local interfacial debonding, which were mainly introduced in the MA process. In contrast, the composite made by MM for 2 h demonstrated high relative density and an excellent thermal conductivity of 3.5 W.m^-1.K^-1, owing to its having few defects and strong inter-facial bonding.

关键词： metal matrix composites thermal properties sintering powder mixing