One-pot Synthesis of 1-Aryloxyacety l-4-(4'-nitrophenyloxyacetyl)-thiosemicarbazides under Phase Transfer Catalysis and Microwave Irradiation

作     者：Zheng LI Xi Cun WANG 

作者机构：College of Chemistry and Chemical EngineeringNorthwest Normal UniversityLanzhou 730070 

出 版 物：《Chinese Chemical Letters》 (中国化学快报(英文版))

年 卷 期：2002年第13卷第8期

页      面：717-720页

核心收录：

学科分类：081704[工学-应用化学] 07[理学] 08[工学] 0817[工学-化学工程与技术] 070303[理学-有机化学] 0703[理学-化学] 

基　　金：Technological Innovation Engineering of Northwest Normal University (NWNU-KJCXGC-218) Natural Science Foundation of Gansu Province and Youth Foundation of Northwest Normal University 

主　　题：Diaryloxyacetyl thiosemicarbazide phase transfer catalysis microwave irradiation. 

摘      要：The 1-aryloxyacetyl-4-(4-nitrophenyloxyacetyl)-thiosemicarbazides (3a-h) are synthe- sized via reaction of 4-nitrophenyloxyacetyl chloride with ammonium thiocyanate and aryloxyacetic hydrazides (2a-h) under phase transfer catalysis and microwave irradiation in excellent yield.