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Effect of Surfactant/Silica and Hydrothermal Time on the Specific Surface Area of Mesoporous Materials from Coal-Measure Kaolin

Effect of Surfactant/Silica and Hydrothermal Time on the Specific Surface Area of Mesoporous Materials from Coal-Measure Kaolin

作     者:吴其胜 WU Qisheng,LI Shuiping (School of Materials Engineering,Yancheng Institute of Technology,Yancheng 224051,China)

作者机构:School of Materials EngineeringYancheng Institute of Technology 

出 版 物:《Journal of Wuhan University of Technology(Materials Science)》 (武汉理工大学学报(材料科学英文版))

年 卷 期:2011年第26卷第3期

页      面:514-518页

核心收录:

学科分类:07[理学] 070205[理学-凝聚态物理] 08[工学] 080501[工学-材料物理与化学] 0805[工学-材料科学与工程(可授工学、理学学位)] 0702[理学-物理学] 

基  金:Funded by Social Development Plan of Jiangsu Department of the Science and Technology Jiangsu China(No.BS2007038) 

主  题:coal measure kaolin mesoporous materials hydrothermal synthesis 

摘      要:Mesoporous materials with the highest surface area were synthesized by hydrothermal treatment from coal-measure kaolin using cetyltrimethylammonium bromide(CTAB)as *** effect of several factors on surface area of products also had been *** products were characterized by FT- IR,HRTEM and N 2 adsorption and desorption isotherm plot *** was typical structure as Si-O,Si- OH and Si-O-Si of mesoporous materials in the framework of synthesized materials;the pore size distributions of the products showed a sharp peak at 3.82 *** effect of hydrothermal treatment time and the amount of template on the specific surface area of mesoporous materials was important,when the Surf/Si=0.135,and hydrothermal time=12 h,and the surface area of the product reached up to 1 070 m2/g,which was higher than other products.

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