Use of Magic Angle Spinning ~1H NMR Spectroscopy to Monitor Reactions in Solid-Phase Synthesis

作     者：Ai Ming YU Hua Zheng YANG(The State Key Laboratory of Elemento-Organic Chemistry, Nankai University, Tianjin 300071)Ping Chuan SUN Zhen Pu ZHANG Ming LI(The State Key Laboratory of Functional Polymeric Materials for Adsorption and Separation,Nankai Uni 

作者机构：State Key Lab. Elemento-Organ. Chem. Nartkai University Tianjin 300071 China State Key Lab. Funct. P.M.A./S. Nankai University Tianjin 300071 China 

出 版 物：《Chinese Chemical Letters》 (中国化学快报（英文版）)

年 卷 期：1997年第8卷第12期

页      面：0-0页

核心收录：

学科分类：081704[工学-应用化学] 07[理学] 08[工学] 0817[工学-化学工程与技术] 070302[理学-分析化学] 0703[理学-化学] 

主　　题：NMR Spectroscopy to Monitor Reactions in Solid-Phase Synthesis Use of Magic Angle Spinning DCC DCM 

摘      要：Proton NMR-spectra of Wang resin bound compounds were obtained using the magic angle spinning 1HNMR technique with standard equipment. It was possible to analyse the spectra to evaluate their utility in solid-phase chernistry. A typical example was presented, which could directly monitor solid-phase reactions