硫化铜纳米粒子的多种制备方法
Methods to Prepare Copper Sulfide Nano-Particles作者机构:后勤工程学院油化系重庆400016
出 版 物:《无机化学学报》 (Chinese Journal of Inorganic Chemistry)
年 卷 期:2001年第17卷第2期
页 面:275-278页
核心收录:
学科分类:081704[工学-应用化学] 07[理学] 070205[理学-凝聚态物理] 08[工学] 0817[工学-化学工程与技术] 080501[工学-材料物理与化学] 0805[工学-材料科学与工程(可授工学、理学学位)] 0703[理学-化学] 070301[理学-无机化学] 0702[理学-物理学]
主 题:纳米粒子 硫源 金属离子螯合剂 制备方法 液相均沉淀法 硫化铜
摘 要:In this paper, Copper sulfide of different size and shape were prepared with three methods by primary materials of Na2S, TAA, EDTA and CuS in water/alcohol (the volume ratio is 3:1 and pH value is 5~7) solution. The synthetic nano-particles were measured by XRD, TEM and IR. The results showed that different synthetic methods affected the size (from 20nm to 50nm or so) and shape (regular ball shape, irregular ball shape and bar shape) of CuS nano-particles. These methods were available for simple synthesis technology, less cost and easily industrial production.