Novel Reaction of Some Azoles with Dimethyl Sulfoxid

作     者：WANG,Bin ZHU,An-Xiong DONG,Heng-Shan 

作者机构：College of Science and Engineering Gansu Association University Lanzhou 730000 Jinchang Agriculture Middle School Gansu 737100 State Key Laboratory of Applied Organic Chemistry Institute of Organic Chemistry College of Chemistry and Chemical Engineering Lanzhou University Lanzhou 730000 

出 版 物：《有机化学》 (Chinese Journal of Organic Chemistry)

年 卷 期：2004年第24卷第Z1期

页      面：146-页

核心收录：

学科分类：07[理学] 070303[理学-有机化学] 0703[理学-化学] 

基　　金：Project supported by the State Key Laboratory of Applied Organic Chemistry  Lanzhou University 

主　　题：spectral data 

摘      要： The compounds 4a～4j were prepared by 3a～3j which were prepared from 1a～1j through 2a～2j. The compounds 6a～6j were prepared by the reaction of the products of 4a～4j with dimethyl sulfoxid via Dimroth rearrangement.[1] The compounds ethyl 5-arylamino-1H-1,2,3-triazol-4-carbonates (5a～5d) and ethyl 2-methylthiamethylene-5-arylamino-2H-1,2,3-triazol-4-carbonates (6a～6j) are established by MS, IR, elemental analysis and 1H NMR spectral data. The route of syntheses is shown in Scheme 1.……