A New Solid Sorbent System for Rapid Monitoring of Dehydrogenated Nicotine by Using Furfural-hydrochloric Acid
A New Solid Sorbent System for Rapid Monitoring of Dehydrogenated Nicotine by Using Furfural-hydrochloric Acid作者机构：School of Studies in Chemistry Pt. Ravishankar Shukla University Raipur (C.G.) 492010 India
出 版 物：《Chinese Chemical Letters》 (中国化学快报（英文版）)
年 卷 期：2006年第17卷第9期
页 面：1267-1270页
核心收录：
学科分类：081704[工学-应用化学] 07[理学] 08[工学] 0817[工学-化学工程与技术] 070303[理学-有机化学] 0703[理学-化学]
基 金：Foundation of Pt. Ravishankar Shukla University and Chattisgarh Council of Science & Technology
主 题：Nicotine solid sorbent system spectrophotometry biological samples.
摘 要：A new solid sorbent system is developed for the monitoring of dehydrogenated nicotine in the environment. The reagent system for the indicator tube consists of furfural-hydrochloric acid and phosphoric acid impregnated over a cellulose fibre （cotton） and a humectant calcium chloride. The reagent system has also been used for the preparation of reagent paper. After exposing the indicator tubes and test paper to dehydrogenated nicotine, for a constant time, the red-violet colour developed could be compared with those obtained from standards. Alternatively the coloured compound was extracted in water and the absorbance measured at 540 nm. The lower limit of detection is 0.03 μg/m^3 of nicotine for the reagent papers and indicator tubes. The lower limit of determination by spectrophotometric procedure is 0.001μg/m^3 of air. The preparation of indicator tubes, test papers and their applications for the detection and determination of nicotine in environmental tobacco smoke （ETS）, mainstream smoke （MS）, side stream smoke （SS） and biological samples is described in this paper.
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