Synthesis of the Complex Fluoride LiBaF_(3) through a Solvothermal Process

作     者：Rui Nian HUA Zhi Hong JIA De Min XIE Chun Shan SHI 

作者机构：Faculty of ChemistryNortheast Normal UniversityChangchun 130024 Key Laboratory of Rare Earth Chemistry and PhysicsChangchun Institute of Applied ChemistryChinese Academy of SciencesChangchun 130022 

出 版 物：《Chinese Chemical Letters》 (中国化学快报(英文版))

年 卷 期：2002年第13卷第10期

页      面：1021-1024页

核心收录：

学科分类：081704[工学-应用化学] 07[理学] 08[工学] 0817[工学-化学工程与技术] 070302[理学-分析化学] 0703[理学-化学] 

基　　金：This work was supported by the State Key Project of Foundation Research (G1998061306) theNational Natural Science Foundation of China (50072031) 

主　　题：Solvothermal synthesis complex fluoride. 

摘      要：The complex fluoride LiBaF3 is solvothermally synthesized at 180degreesC and characterized by means of X-ray powder diffraction, scanning electron microscopy, thermogravimetric analysis and infrared spectroscopy. In the solvothermal process, the solvents, mole ratios of initial mixtures and reaction temperature play important roles in the growth of the single crystal.