Synthesis and Characterization of New Schiff Bases Formed by Condensation of 2,9-Phenathroline-1,10-dialdehyde with Sulfur-Containing Amines
Synthesis and Characterization of New Schiff Bases Formed by Condensation of 2,9-Phenathroline-1,10-dialdehyde with Sulfur-Containing Amines作者机构:Department of Chemistry Tennessee State University Nashville USA Faculty of Science University of Brunei Darussalam Bandar Seri Begawan Brunei.
出 版 物:《International Journal of Organic Chemistry》 (有机化学国际期刊(英文))
年 卷 期:2013年第3卷第1期
页 面:81-86页
主 题:Phenanthroline Schiff Base Dithiocarbazide Sulfur-Containing Antibaterial
摘 要:Four new Schiff bases of 1,10-phenanthroline-2,9-dicarboxaldehyde with sulfur-containing amines such as 2-mercaptoaniline, S-alkyl/aryl dithiocarbazates and thiosemicarbazide have been synthesized and characterized by spectroscopic and X-ray crystallographic techniques. A comparative study of the methods of synthesis has been made using both traditional and microwave techniques. A significant reduction in reaction time has been observed when the microwave method was used. In some of the reactions, the yields also increased significantly.