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Synthesis of Mesoporous Material from Chrysotile-Derived Silica

合成介孔材料从温石棉派生二氧化硅

作     者:Anderson Joel Schwanke Christian Wittee Lopes Sibele Berenice Castella Pergher 

作者机构:PPGCEMUniversidade Federal do Rio Grande do NorteNatalBrazil Chemistry InstituteUniversidade Federal do Rio Grande do NorteNatalBrazil 

出 版 物:《Materials Sciences and Applications》 (材料科学与应用期刊(英文))

年 卷 期:2013年第4卷第8期

页      面:68-72页

学科分类:07[理学] 0703[理学-化学] 

基  金:The authors gratefully acknowledge financial support from CAPES organization as well as the NEPGN-UFRN organization for use of their Scanning Electron Micros-copy 

主  题:MCM-41 Chrysotile Silica Source 

摘      要:Mesoporous MCM-41-type molecular sieves were synthesized using calcined and leached chrysotile and cetyltrimethylammonium bromide as the silica source and structure directing agent, respectively. Powder X-ray diffraction (XRD), N2 isothermal adsorption-desorption, scanning electron microscopy (SEM) and thermogravimetric analysis (TGA) were used to characterize the samples. The calcined and leached chrysotile can be employed as an inexpensive silica source for the formation of low-order MCM-41 mesoporous materials.

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