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Li<SUB>4</SUB>Ti<SUB>5</SUB>O<SUB>12</SUB>Synthesis with High Specific Surface Area and Single Phase

Li<SUB>4</SUB>Ti<SUB>5</SUB>O<SUB>12</SUB>Synthesis with High Specific Surface Area and Single Phase

作     者:Toshihito Ohtake Ken-ichiro Iijima 

作者机构:Department of Mechanical Systems Engineering Faculty of Engineering Aich University of Technology Gamagori Japan 

出 版 物:《Journal of Materials Science and Chemical Engineering》 (材料科学与化学工程(英文))

年 卷 期:2015年第3卷第9期

页      面:68-73页

学科分类:07[理学] 0703[理学-化学] 

主  题:Li4Ti5O12 Solid Phase Synthesis Specific Surface Area SEM TEM 

摘      要:We have investigated a novel Li4Ti5O12 synthesis with high specific surface area, high crystallization and single phase and its mechanism. The method was performed with a solid phase synthesis by using CH3COOLi·2H2O and anatase TiO2 via Li2TiO3 as an intermediate in pre-sintering at 500°C and sintering at 750°C. This result showed specific surface area of 12 m2/g and single phase- Li4Ti5O12 by applying the high specific surface anatase TiO2 as a precursor.

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