Effect of inductively coupled plasma surface treatment on silica gel and mesoporous MCM-41 particles

作     者：J A JUAREZ-MORENO U CHACON-ARGAEZ J BARRON-ZAMBRANO C CARRERA-FIGUEIRAS P QUINTANA-OWEN W TALAVERA-PECH Y PEREZ-PADILLA A AVILA-ORTEGA 

作者机构：facultad de ingeniería química-uadyperiférico norte kilómetro 33.5col.chuburna de hidalgo inn C.P. 97203 Mérida Yucatan México centro de investigación y de estudios avanzados del ipn-unidad mérida km.6 antigua carretera a progreso apdo. Postal 73 Cordemex 97310 Méfida Yucatán México 

出 版 物：《Plasma Science and Technology》 (等离子体科学和技术（英文版）)

年 卷 期：2018年第20卷第6期

页      面：104-113页

核心收录：

学科分类：07[理学] 0805[工学-材料科学与工程（可授工学、理学学位）] 070204[理学-等离子体物理] 0702[理学-物理学] 

基　　金：supported by CONACYT Ciencia Básica project 176544 SEM and XPS measurements were performed at LANNBIO Cinvestav Mérida,under support from projects FOMIX-Yucatán 2008-108160,CONACYT LAB2009-01 No.123913 

主　　题：silica MCM-41 nanoparticles plasma treatment 

摘      要：Silica gel and MCM-41 synthesized mesoporous materials were treated with either oxygen（O_2）,hexamethyldisiloxane（HMDSO） and organic vapors like ethanol（Et OH）,and acrylonitrile（AN）inductive *** radiofrequency power for the modification was fixed to 120 W and30 min,assuring a high degree of organic ionization energy in the *** surface properties were studied by infrared spectroscopy（FTIR）,scanning electron microscopy,x-ray photoelectron spectroscopy and dynamic light scattering technique was used for characterizing size *** the silica and MCM-41 particles were modified by AN and HMDSO plasma gases,the surface morphology of the particles was changed,presenting another color,size or *** contrast,the treatments of oxygen and Et OH did not affect the surface morphology of both particles,but increased the oxygen content at the surface bigger than the AN and HMDSO plasma *** this study,we investigated the influence of different plasma treatments on changes in morphology and the chemical composition of the modified particles which render them a possible new adsorbent for utilization in sorptive extraction techniques for polar compounds.