Preparation of copper nano-particle powder by γ-irradiation
Preparation of copper nano-particle powder by γ-irradiation作者机构:Institute of Nuclear Agricultural Sciences Zhejiang University Hangzhou 310021 China Energy and Nuclear Technology Application Institute Hangzhou 310012 China
出 版 物:《Nuclear Science and Techniques》 (核技术(英文))
年 卷 期:2012年第23卷第3期
页 面:163-168页
核心收录:
学科分类:080503[工学-材料加工工程] 081704[工学-应用化学] 07[理学] 08[工学] 0817[工学-化学工程与技术] 0805[工学-材料科学与工程(可授工学、理学学位)] 0703[理学-化学] 070301[理学-无机化学]
主 题:铜纳米颗粒 制备 粉末 表面活性剂 铜纳米粒子 透射电子显微镜 差示扫描量热法 激光粒度分析仪
摘 要:Copper nano-particles were prepared by 100 kGy room temperature γ-ray irradiation of CuSO4 aqueous solution added with surfactant and inactive *** of the surfactants and pH value on particle size and morphology of the Cu powder,and the storage stability,were ***,morphology,particle size and melting point of the copper nano-particles were characterized by X-ray diffraction(XRD),transmission electron microscopy(TEM),laser particle size analyzer and differential scanning calorimetry(DSC),*** results show that the Cu nano-particles prepared with PCM as surfactant and N,N-bis-hydroxyethyl dodecyl amide as inactive agent,in pH=4.0-6.5 of the aqueous solution,can be stored in air for 140 days.