THE STRUCTURE OF BIS （TETRAETHYLAMMONIUM）（DICHLORODITHIOFERRATO- S,S’）-DIOXOMOLYBDATE, （Et4N）2[Cl2FeS2MoO2]

作     者：Cai Jinhua Cheng ChangnengFujian Institute of Research on the Structure of Matter, Academia Sinica Cai Jinhua Cheng ChangnengFujian Institute of Research on the Structure of Matter, Academia Sinica

出 版 物：《结构化学》 (Chinese Journal of Structural Chemistry)

年 卷 期：1985年第2期

页      面：100-102页

学科分类：07[理学] 0703[理学-化学] 

主　　题：FeS Mo Et4N DICHLORODITHIOFERRATO TETRAETHYLAMMONIUM S,S DIOXOMOLYBDATE THE STRUCTURE OF BIS Cl2FeS2MoO2 

摘      要：(Et4N)2[Cl2FeS2MoO2], Mr = 579.3, monoclinic, P21, a = 13.531(2) b = 8.912(2), c = 11.095(2)A, β= 95.39(4)°, V r 1331.9(8)A3, Z = 2, DC =1.444 gcm-3, MoK , radiation, λ= 0.71069A, R = 0.065 for 1725 observed reflections. The complex anion (OaMoSzFeCl2)2- contains a cluster core (MoS2Fe) with the Mo-Fe distance of 2.859A.