Separation,preconcentration and determination of Pb(Ⅱ) in water samples using microcrystalline triphenylmethane loaded with quinolin-8-olate

作     者：Li Na Hu Zhao Gang Ren 

作者机构：College of Chemistry and Chemical Engineering China West Nomal University Nanchong 637002 China 

出 版 物：《Chinese Chemical Letters》 (中国化学快报（英文版）)

年 卷 期：2009年第20卷第3期

页      面：334-338页

核心收录：

学科分类：12[管理学] 1204[管理学-公共管理] 082803[工学-农业生物环境与能源工程] 081704[工学-应用化学] 07[理学] 08[工学] 0817[工学-化学工程与技术] 0828[工学-农业工程] 070303[理学-有机化学] 0703[理学-化学] 120405[管理学-土地资源管理] 

主　　题：Microcrystalline triphenylmethane Quinolin-8-olate Separation Preconcentration and determination 

摘      要：This paper described a novel method for the preconcentration of Pb（II） using microcrystalline triphenylmethane loaded with quinolin-8-olate prior to the determination by flame atomic absorption spectrometry. Pb（II） could be enriched by controlling appropriate condition. The preconcentration factor could reach to 200 and the detection limit of Pb（II） was 0.074 μg/L. The recovery was in a range of 93.5-103% with relative standard deviation of 1.0-2.2%. The proposed method had been successfully applied to the determination of trace Pb（U） in various water samples with satisfactory result.