Synthesis of Gd_2O_3 nanoparticles:using bulk Gd_2O_3 powders as precursor
Synthesis of Gd_2O_3 nanoparticles:using bulk Gd_2O_3 powders as precursor作者机构:Nuclear Fuel Cycle Research School Nuclear Science andTechnology Research Institute
出 版 物:《Rare Metals》 (稀有金属(英文版))
年 卷 期:2015年第34卷第8期
页 面:540-545页
核心收录:
学科分类:07[理学] 0806[工学-冶金工程] 070205[理学-凝聚态物理] 08[工学] 080501[工学-材料物理与化学] 0805[工学-材料科学与工程(可授工学、理学学位)] 0703[理学-化学] 0702[理学-物理学]
基 金:financially supported by the Nuclear Science and Technology Research Institute of Iran
主 题:Gd2O3 Nanoparticles Electro-deposition Nanostructu
摘 要:Gd2O3nanoparticles were synthesized from the commercial bulk Gd2O3 powders via a simple electrochemical method. The synthesized powders were characterized by means of X-ray powder diffraction(XRD),scanning electron microscopy(SEM), transmission electron microscopy(TEM) and Fourier transform infrared(FTIR) spectroscopy. The effects of solution p H on the morphological features of the sample were studied. The strategy developed in this study offers significant advantages for the synthesis of Gd2O3 nanoparticles from the bulk Gd2O3 powders compared with the conventional routes. From SEM observations, the size of the Gd2O3 nanoparticles is estimated to be significantly smaller than70 nm.