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Additive-free synthesis of β-keto phosphorodithioates via geminal hydro-phosphorodithiolation of sulfoxonium ylides with P_(4)S_(10)and alcohols

作     者:Jindong Hao Yufen Lv Shuyue Tian Chao Ma Wenxiu Cui Huilan Yue Wei Wei Dong Yi Jindong Hao;Yufen Lv;Shuyue Tian;Chao Ma;Wenxiu Cui;Huilan Yue;Wei Wei;Dong Yi

作者机构:Key Laboratory of Catalytic Conversion and Clean Energy in Universities of Shandong ProvinceSchool of Chemistry and Chemical EngineeringQufu Normal UniversityQufu 273165China Qinghai Provincial Key Laboratory of Tibetan Medicine Research and CAS Key Laboratory of Tibetan Medicine ResearchNorthwest Institute of Plateau BiologyXining 810008China Green Pharmaceutical Technology Key Laboratory of Luzhou CitySchool of PharmacySouthwest Medical UniversityLuzhou 646000China 

出 版 物:《Chinese Chemical Letters》 (中国化学快报(英文版))

年 卷 期:2024年第35卷第9期

页      面:165-168页

核心收录:

学科分类:081704[工学-应用化学] 07[理学] 08[工学] 0817[工学-化学工程与技术] 070303[理学-有机化学] 0703[理学-化学] 

基  金:supported by the Natural Science Foundation of Shandong Province(No.ZR2021MB065) Scientific Research Startup Foundation of Qufu Normal University and National Natural Science Foundation of China(No.22101237) 

主  题:β-Keto phosphorodithioates Phosphorodithiolation Sulfoxonium ylides P_(4)S_(10) Alcohols 

摘      要:A simple and additive-free protocol has been developed for the preparation ofβ-keto phosphorodithioates through the three-component reaction of easily available sulfoxonium ylides,P_(4)S_(10),and *** present geminal hydro-phosphorodithiolation reaction was performed at room temperature to construct a series ofβ-keto phosphorodithioates in the absence of any metal reagents,bases,or additives.

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