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Development of In Situ MAS NMR and Its Applications in Material Synthesis and Heterogeneous Catalysis

Development of In Situ MAS NMR and Its Applications in Material Synthesis and Heterogeneous Catalysis

作     者:Xinlong Yao Zhenchao Zhao Guangjin Hou Xinlong Yao;Zhenchao Zhao;Guangjin Hou

作者机构:State Key Laboratory of CatalysisDalian National Laboratory for Clean Energy2011-Collaborative Innovation Center of Chemistry for Energy MaterialsDalian Institute of Chemical PhysicsChinese Academy of SciencesDalian 116023China University of Chinese Academy of SciencesBejing 100049China Key Laboratory of the Ministry of Education for Advanced Catalysis MaterialsInstitute of Physical ChemistryZhejiang Normal UniversityJinhua 321004China 

出 版 物:《Chinese Journal of Structural Chemistry》 (结构化学(英文))

年 卷 期:2022年第41卷第10期

页      面:45-55页

核心收录:

学科分类:081705[工学-工业催化] 08[工学] 0817[工学-化学工程与技术] 080501[工学-材料物理与化学] 0805[工学-材料科学与工程(可授工学、理学学位)] 0703[理学-化学] 

基  金:the financial supports from the National Natural Science Foundation of China(Nos.21773230,91945302 and 21972143) the National Key R&D Program of China(2021YFA1502803) Liao Ning Revitalization Talents Program(XLYC1807207) DICP&QIBEBT UN201808 DICP I202104 

主  题:in situ NMR high-temperature high-pressure material synthesis heterogeneous catalysis molecular sieves 

摘      要:High-resolution magic angle spinning(MAS)NMR can afford both qualitative and quantitative information of the solid,liquid and gas phase at atomic level,and such information obtained at in situ/operando conditions is of vital importance for understanding the crystallization process of material as well as the reaction mechanism of *** meet the requirement of experimental conditions for material synthesis and catalytic reactions,in situ MAS NMR techniques have been continuously developed for using at higher temperatures and pressures with high ***,we will briefly outline the development of this technology and discuss its detailed applications in understanding material synthesis and heterogeneous catalysis.

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