静电纺丝法制备ZrO_2纳米纤维
Fabrication of ZrO_2 Nanofibers by Electrospinning作者机构:东北师范大学先进光电子功能材料研究中心长春130024
出 版 物:《高等学校化学学报》 (Chemical Journal of Chinese Universities)
年 卷 期:2004年第25卷第8期
页 面:1413-1415,M009页
核心收录:
学科分类:07[理学] 0703[理学-化学] 070301[理学-无机化学]
基 金:教育部科学技术研究重点项目 (批准号 :10 40 71) 吉林省科技厅自然科学基金(批准号 :2 0 0 2 0 613 )资助
摘 要:Thin PVA/zirconium oxychloride composite fibers were prepared by using sol-gel processing and electrospinning technique. After calcining the above precursor fibers,ZrO 2 nanofibers with a diameter of 70—100 nm were successfully obtained. The ZrO 2 nanofibers were characterized by XRD,TG-DTA,FTIR,and SEM,respectively. The results show that the crystallinity and morphology of ZrO 2 fibers are largely influenced by the calcination temperature.